取向銥單晶柱為材料,進(jìn)行了單軸壓縮試驗(yàn)。實(shí)驗(yàn)在納米機(jī)械儀器Sementort中進(jìn)行,結(jié)果表明,單晶柱的屈服強(qiáng)度與直徑有顯著關(guān)系,而與FIB制備無(wú)關(guān)。單晶柱的微壓縮實(shí)驗(yàn)與整體銥在單軸壓縮試驗(yàn)中的力學(xué)行為不同,微納米尺度的流動(dòng)應(yīng)力隨著柱直徑的減小而增加,即尺寸效應(yīng)。此外,塑性變形過(guò)程有明顯的突變和大應(yīng)變,重點(diǎn)研究了單軸壓縮下銥單晶柱的應(yīng)變突變的速度和應(yīng)變敏感性問(wèn)題。結(jié)果表明,壓縮位移量隨著持續(xù)時(shí)間和立柱直徑的增加而增加,同時(shí)指出了應(yīng)變敏感性( SRS )指數(shù)m,其值隨著柱直徑的減小而增加。"/>

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關(guān)于銥微柱的應(yīng)變突變和應(yīng)變速率敏感性問(wèn)題研究
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昆明貴金屬研究所鉑族金屬綜合利用先進(jìn)技術(shù)國(guó)家重點(diǎn)實(shí)驗(yàn)室

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國(guó)家自然科學(xué)基金項(xiàng)目(面上項(xiàng)目,重點(diǎn)項(xiàng)目,重大項(xiàng)目)


Strain burst and strain rate sensitivity of iridium micro-pillars
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State Key Laboratory of Advanced Technologies for Comprehensive Utilization of Platinum Metal,Kunming Institute of Precious Metals

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    以聚焦離子束( FIB )制備的直徑在1000 nm至7400 nm范圍內(nèi)的< 110 >取向銥單晶柱為材料,進(jìn)行了單軸壓縮試驗(yàn)。實(shí)驗(yàn)在納米機(jī)械儀器Sementort中進(jìn)行,結(jié)果表明,單晶柱的屈服強(qiáng)度與直徑有顯著關(guān)系,而與FIB制備無(wú)關(guān)。單晶柱的微壓縮實(shí)驗(yàn)與整體銥在單軸壓縮試驗(yàn)中的力學(xué)行為不同,微納米尺度的流動(dòng)應(yīng)力隨著柱直徑的減小而增加,即尺寸效應(yīng)。此外,塑性變形過(guò)程有明顯的突變和大應(yīng)變,重點(diǎn)研究了單軸壓縮下銥單晶柱的應(yīng)變突變的速度和應(yīng)變敏感性問(wèn)題。結(jié)果表明,壓縮位移量隨著持續(xù)時(shí)間和立柱直徑的增加而增加,同時(shí)指出了應(yīng)變敏感性( SRS )指數(shù)m,其值隨著柱直徑的減小而增加。

    Abstract:

    The current study presents a uniaxial compression testing of <110>-oriented single-crystalline Iridium micropillars with diameters ranging from 1000 nm to 7400 nm fabricated by focused-ion-beam (FIB). The tests were performed on a nanomechanical instrument. The results reveal that the yield strength of micropillars follow a power law depending on diameter, as reported in other face-centered cubic (FCC) metals. Unlike the mechanical behavior of bulk Iridium when performing uniaxial compression, the flow stress at micro- and nano-scale is found to increase with a decreasing of micropillar diameter, which is attributed to a size-dependent effect. Moreover, the plastic deformation shows a periodical jerky and strain bursts. This work mainly focused on the rate of strain bursts and the sensitivity of strain rate in Iridium micropillars under uniaxial compression. The experiments also indicate that the displacement jumps increase with the extending of durations and micropillar diameter. In addition, the strain rate sensitivity (SRS) index m increases with a decreasing diameter of Iridium micropillar.

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劉毅,李揚(yáng),羅錫明,張健康,許昆,李偉.關(guān)于銥微柱的應(yīng)變突變和應(yīng)變速率敏感性問(wèn)題研究[J].稀有金屬材料與工程,2020,49(4):1200~1203.[Yi Liu, Yang Li, Xi-Ming Luo, Jian-Kang Zhang, Kun Xu, Wei Li. Strain burst and strain rate sensitivity of iridium micro-pillars[J]. Rare Metal Materials and Engineering,2020,49(4):1200~1203.]
DOI:10.12442/j. issn.1002-185X.20181242

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  • 收稿日期:2018-12-12
  • 最后修改日期:2020-04-07
  • 錄用日期:2019-02-20
  • 在線(xiàn)發(fā)布日期: 2020-05-07
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