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半固態(tài)熱等靜壓Al/B4C復(fù)合材料液相流動(dòng)行為與致密化機(jī)理
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中國(guó)工程物理研究院

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國(guó)家高技術(shù)研究發(fā)展計(jì)劃(863計(jì)劃),國(guó)家自然科學(xué)基金項(xiàng)目(面上項(xiàng)目,重點(diǎn)項(xiàng)目,重大項(xiàng)目)


Liquid Phase Flow Behavior and Densification Mechanism of Al/B4C Composites Fabricated via Semisolid Hot Isostatic Pressing
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China Academy Engineering Physics,Mianyang

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The National High Technology Research and Development Program of China (863 Program), The National Natural Science Foundation of China (General Program, Key Program, Major Research Plan)

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    摘要:

    鋁基碳化硼復(fù)合材料是一種重要的中子吸收材料。為了制備具有更高密度的鋁基碳化硼材料,研究采用粉末冶金半固態(tài)熱等靜壓方法制備了含量為30%碳化硼的鋁基碳化硼材料,采用WANCE100型材料力學(xué)性能試驗(yàn)機(jī)和SIRION200型掃描電鏡研究了復(fù)合材料的力學(xué)性能及顯微形貌。結(jié)果表明:半固態(tài)熱等靜壓工藝可制備獲得接近理論密度的Al/B4C復(fù)合材料;雖然Al/B4C材料抗拉強(qiáng)度可提升至約300Mpa,但過高碳化硼含量也使得該材料脆性特征十分明顯;研究同時(shí)采用間接的方法觀察到了半固態(tài)工藝過程中生成的液相,該液相不僅可改善碳化硼顆粒與鋁基體的結(jié)合性,在高溫高壓下液相的流動(dòng)還起到填充復(fù)合材料內(nèi)部空隙的作用。半固態(tài)熱等靜壓工藝過程中產(chǎn)生的液相是復(fù)合材料密度和機(jī)械性能提升的主要原因。

    Abstract:

    Aluminum matrix Boron carbide (Al/B4C) composites is an important thermal neutron shielding material. In order to prepare B4C/6061Al composite with higher density, Al/B4C composites reinforced by 30wt.% B4C particle were fabricated via hot isostatic pressing in the semi-solid temperature range of 6061Al. Microstructures, mechanical properties and densification mechanism of the composites were investigated. The results indicate that the density of Al/B4C composite is very close to the theoretical density with the usage of semisolid hot isostatic pressing. Although the tensile strength can reach up to 300 MPa, the ductility of the semisolid HIP Al/B4C composite is not good mainly because of the high content of 30wt%B4C. Aluminum liquid phase is observed indirectly which mainly formed during semisolid temperature range of 6061Al, it is helpful to improve the combination between the B4C particles and the 6061Al matrix. The increasing of density and Strength property mainly also due to the effect of aluminum liquid flows into the internal gaps under the hot isostatic pressing condition with high temperature and high pressure.

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龐曉軒,鮮亞疆,羅昊,張佳佳,張鵬程.半固態(tài)熱等靜壓Al/B4C復(fù)合材料液相流動(dòng)行為與致密化機(jī)理[J].稀有金屬材料與工程,2019,48(10):3102~3107.[Xiaoxuan Pang, Yajiang Xian, Hao Luo, Jiajia Zhang, Pengcheng Zhang. Liquid Phase Flow Behavior and Densification Mechanism of Al/B4C Composites Fabricated via Semisolid Hot Isostatic Pressing[J]. Rare Metal Materials and Engineering,2019,48(10):3102~3107.]
DOI:10.12442/j. issn.1002-185X.20180393

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  • 收稿日期:2018-04-18
  • 最后修改日期:2018-05-18
  • 錄用日期:2018-05-21
  • 在線發(fā)布日期: 2019-11-01
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