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熱處理溫度對半固態(tài)擠壓錫青銅組織性能的影響
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昆明理工大學(xué)材料科學(xué)與工程學(xué)院

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Effect of heat treatment temperature on microstructure and mechanical properties of semi-solid extruded tin bronze
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Faculty of Materials Science and Engineering,Kunming University of Science and Technology

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    摘要:

    本文以半固態(tài)擠壓ZCuSn10P1錫青銅為研究對象,采用光學(xué)顯微鏡、掃描電鏡、顯微硬度儀、布氏硬度計(jì)、拉伸試驗(yàn)機(jī)研究了熱處理溫度對半固態(tài)擠壓錫青銅微觀組織和力學(xué)性能的影響規(guī)律。結(jié)果表明:熱處理對半固態(tài)擠壓錫青銅強(qiáng)度、硬度和組織影響較大。當(dāng)熱處理溫度由250℃升高至650℃時(shí),錫青銅抗拉強(qiáng)度先增加后降低,延伸率增加;布氏硬度先增加后降低;固相和固液界面顯微硬度增加,液相顯微硬度降低;固相平均晶粒尺寸增加,但熱處理溫度650℃時(shí)組織已不是球狀而變成薔薇狀。隨溫度增加,固相中Sn和P元素增加,元素偏析減弱。綜合性能較佳的熱處理工藝為350℃保溫120min,此時(shí)錫青銅抗拉強(qiáng)度為402 MPa,延伸率為4.5%,布氏硬度為136HBW,與未熱處理前分別提高了3.88%、60.71%、6.25%。

    Abstract:

    The semi-solid extruded ZCuSn10P1 tin bronze was used as the research object. The effects of heat treatment temperature on microstructure and mechanical properties of semi-solid extruded tin bronze were investigated by using optical microscopy, scanning electron microscopy, microhardness test, Brinell hardness test, tensile test machine. The results indicate that the heat treatment has a great effect on the strength, hardness and microstructure of semi-solid extruded tin bronze. With the heat treatment temperature increase from 250℃ to 650℃, the tensile strength of tin bronze increases first and then decreases, the elongation increases, the Brinell hardness increases first and then decreases. The Vickers hardness of the solid zone and solid-liquid interface increases, however, the liquid zone decreases. The average grain size of solid phase increases, while it is not spherical but rose-like with the temperature increases up to 650°C. With the increase of temperature, the element contents of Sn and P in the solid phase increase, and element segregation weakens. The comprehensive mechanical properties of tin bronze at heat treatment temperature 350°C for 120 min are fine. At this time, the tensile strength is 402 MPa, elongation is 4.5%, Brinell hardness is 136 HBW, compared with before heat treatment, it increases by3.88%, 60.71%, and 6.25%, respectively.

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肖 寒,段志科,李乃擁,熊 遲,周榮鋒,盧德宏,蔣業(yè)華.熱處理溫度對半固態(tài)擠壓錫青銅組織性能的影響[J].稀有金屬材料與工程,2019,48(1):235~241.[Xiao Han, Duan Zhike, Li Naiyong, Xiong Chi, Zhou Rongfeng, Lu Dehong, Jiang Yehua. Effect of heat treatment temperature on microstructure and mechanical properties of semi-solid extruded tin bronze[J]. Rare Metal Materials and Engineering,2019,48(1):235~241.]
DOI:10.12442/j. issn.1002-185X.20180377

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  • 收稿日期:2018-04-16
  • 最后修改日期:2018-05-03
  • 錄用日期:2018-06-15
  • 在線發(fā)布日期: 2019-02-18
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