-1/s降至6.94×10-2/s時(shí)再結(jié)晶晶粒面積占比減小,而當(dāng)應(yīng)變率從6.94×10-2/s進(jìn)一步降至6.94×10-3/s時(shí),再結(jié)晶晶粒面積占比顯著提高。"/>

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Al-10Mg 合金熱壓縮過程中項(xiàng)鏈組織的形成和擴(kuò)展行為
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清華大學(xué)材料學(xué)院先進(jìn)材料教育部重點(diǎn)實(shí)驗(yàn)室

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國家國際科技合作專項(xiàng)項(xiàng)目(NO. 2015DFR50470)


Necklace Structure Formation and Expansion Behavior In an Al-10Mg Alloy During Hot Uniaxial Compression
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School of Material Science and Engineering,Tsinghua University

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the International Science & Technology Cooperation Program of China (2015DFR50470)

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    摘要:

    本文采用旋轉(zhuǎn)結(jié)晶工藝制備高鎂含量的Al-10Mg合金坯料、并對(duì)其進(jìn)行673K/24h固溶處理及單軸熱壓縮變形。通過流變應(yīng)力行為及微觀組織表征來分析合金動(dòng)態(tài)再結(jié)晶過程中項(xiàng)鏈組織的形核及擴(kuò)展行為,特別地,分析了變形溫度和應(yīng)變率對(duì)項(xiàng)鏈組織擴(kuò)展行為的不同影響。研究表明:大角度晶界的凸出是項(xiàng)鏈組織首層再結(jié)晶晶粒的形核方式, Al-10Mg合金變形組織中有微帶、應(yīng)變誘發(fā)的小角度晶界和回復(fù)形成的小角度晶界等三種亞晶界。隨變形溫度升高,微帶和回復(fù)形成的小角度晶界逐漸消失,應(yīng)變誘發(fā)的小角度晶界形核及由大角度晶界遷移造成的再結(jié)晶晶粒粗化是項(xiàng)鏈組織擴(kuò)展的主要方式;隨應(yīng)變率的降低,未再結(jié)晶的變形晶粒被劃分為低取向差中心區(qū)、外層再結(jié)晶晶粒區(qū)和處于中間層的富集小角度晶界的網(wǎng)狀結(jié)構(gòu)區(qū)等三部分,應(yīng)變率從6.94×10-1/s降至6.94×10-2/s時(shí)再結(jié)晶晶粒面積占比減小,而當(dāng)應(yīng)變率從6.94×10-2/s進(jìn)一步降至6.94×10-3/s時(shí),再結(jié)晶晶粒面積占比顯著提高。

    Abstract:

    The formation and expansion of necklace structure in an Al-10Mg alloy have been studied. The alloy was produced by centrifugal casting, which was followed by 673K/24h solid solution treatment and hot uniaxial compression. The different effects of temperature and strain rate on expansion of necklace structure were especially clarified. In this study, bulging is the nucleation type of first layer in necklace structure, and three different types of subboundary were found in the deformation microstructure of Al-10Mg alloy. When temperature increased, microband and recovered subboundary were gradually eliminated, after which strain-induced subboundary nucleation and recrystallized grain coarsening became a main way of necklace expansion. When strain rate decreased, low angle grain boundary was accumulated. Three regions denoted by low misorientation region in interior, new grains in out layer and net structure of subboundary concentration region in middle were observed in non-recrystallized grains. The proportion of recrystallized grain area decreased when strain rate changed from 6.94×10-1/s to 6.94×10-2/s, then significantly increased when strain rate changed from 6.94×10-2/s to 6.94×10-3/s.

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毛軼哲,李建國,李聰,封蕾. Al-10Mg 合金熱壓縮過程中項(xiàng)鏈組織的形成和擴(kuò)展行為[J].稀有金屬材料與工程,2019,48(9):2729~2736.[Mao Yizhe, Li Jianguo, Li Cong, Feng Lei. Necklace Structure Formation and Expansion Behavior In an Al-10Mg Alloy During Hot Uniaxial Compression[J]. Rare Metal Materials and Engineering,2019,48(9):2729~2736.]
DOI:10.12442/j. issn.1002-185X.20180344

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  • 收稿日期:2018-04-08
  • 最后修改日期:2018-05-05
  • 錄用日期:2018-05-18
  • 在線發(fā)布日期: 2019-10-09
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