方向的擇優(yōu)取向;隨著應變的增加,擇優(yōu)取向消失,組織趨于均勻。應變較高(扭轉5圈)時在三叉晶界處出現(xiàn)了細小的動態(tài)再結晶晶粒。高壓扭轉變形引起的孔隙閉合、晶粒細化、晶格畸變、位錯密度增加和大角度晶界形成,導致屈服強度和納米硬度隨變形量的增大而不斷提升;而在致密度、殘余內應力和高密度位錯的共同作用下,變形試樣的彈性模量顯著高于工業(yè)燒結純鎢,但隨著應變量的增大略有降低。"/>

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純鎢高壓扭轉組織與性能的微觀尺度分析
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材料科學與工程學院

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中圖分類號:

TG311

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國家自然科學基金資助(項目號51675154,51705118)


Study on Microstructure Evolution and Micro-mechanical Properties of Pure Tungsten During High Pressure Torsion
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School of Materials Science and Engineering,Hefei University of Technology,Hefei,Anhui,230009

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    摘要:

    采用高壓扭轉技術在550 ℃、1.5 GPa壓力下成功制得具有細晶組織的難熔金屬鎢,借助EBSD技術研究了高壓扭轉變形組織晶粒尺寸、晶界角度以及晶粒取向的演化規(guī)律,結合納米壓痕實驗結果,分析了應變對工業(yè)燒結純鎢微觀力學性能的影響機理。實驗結果表明,高壓扭轉后材料內部微孔隙有效閉合,組織細化顯著,大角度晶界含量快速升高。在應變較低時出現(xiàn)較為明顯的沿<101>方向的擇優(yōu)取向;隨著應變的增加,擇優(yōu)取向消失,組織趨于均勻。應變較高(扭轉5圈)時在三叉晶界處出現(xiàn)了細小的動態(tài)再結晶晶粒。高壓扭轉變形引起的孔隙閉合、晶粒細化、晶格畸變、位錯密度增加和大角度晶界形成,導致屈服強度和納米硬度隨變形量的增大而不斷提升;而在致密度、殘余內應力和高密度位錯的共同作用下,變形試樣的彈性模量顯著高于工業(yè)燒結純鎢,但隨著應變量的增大略有降低。

    Abstract:

    Near-equiaxed fine grains with the average grain size of 1.21 μm of pure tungsten has been fabricated via high pressure torsion (HPT) at the temperature of 550 ℃, under a pressure of 1.5 GPa. The influence of HPT processing at various turning numbers on microstructure and micro-mechanical properties of sintered commercial pure tungsten has been investigated by means of EBSD and nano-indentation experiments. It was found that the pores in material were closed effectively, the grains were refined significantly and the ratio of high angle boundary increased rapidly after HPT processing. Moreover, when the strain was relatively low (at the turning number of 1), there was a preferred grain orientation along <101>, which weakened to disappearing with the strain increasing; when the strain was high (at the turning number of 5), some small dynamic recrystallites generated at grain boundary. In addition, the nanohardness and yield strength increase obviously as the strain increasing, which is due to pores closure, grain refinement, lattice distortion, dislocation density increase and high angle grain boundary formation; the combination of relative density, residual stress and high density dislocation, make the elastic modulus of HPT-processed samples higher than sintered commercial pure tungsten, but decrease slightly as the strain increasing during the processing.

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李 萍,華雅玲,林泉,王雪,薛克敏.純鎢高壓扭轉組織與性能的微觀尺度分析[J].稀有金屬材料與工程,2019,48(7):2220~2224.[Ping Li, Yaling Hua, Quan Lin, Xue Wang, Kemin Xue. Study on Microstructure Evolution and Micro-mechanical Properties of Pure Tungsten During High Pressure Torsion[J]. Rare Metal Materials and Engineering,2019,48(7):2220~2224.]
DOI:10.12442/j. issn.1002-185X.20180123

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  • 收稿日期:2018-02-01
  • 最后修改日期:2018-02-07
  • 錄用日期:2018-03-12
  • 在線發(fā)布日期: 2019-08-01
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