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熱暴露對表面預(yù)形變單晶合金組織和性能的影響
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中國航發(fā)北京航空材料研究院

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航空基金(2015ZF21017)


Effect of Thermal Exposure on the Micro-structure and Performance of Surface Pre-deformed Single-crystal Superalloy
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AECC Beijing Institute of Aeronautical Materials

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    摘要:

    針對[001]取向的DD11單晶合金,垂直于[001]方向進(jìn)行兩種強(qiáng)度的鑄鋼彈丸噴丸強(qiáng)化以引入表面預(yù)形變,采用電子背散射衍射(EBSD)、掃描電鏡和硬度等方法研究了預(yù)形變后表層組織;后續(xù)熱暴露完成后,采用掃描電鏡和硬度計(jì),研究了熱暴露溫度和預(yù)形變程度對表層組織和硬度梯度的共同影響;并且表征了噴丸+熱暴露后單晶合金的高溫疲勞性能。結(jié)果表明,單晶合金噴丸預(yù)形變后表面出現(xiàn)[110]和[111]取向的亞晶,同時(shí)出現(xiàn)表面應(yīng)變硬化效果;隨著形變程度的增大,亞晶取向角、旋轉(zhuǎn)亞晶層深度和硬化效果也隨之增大。隨著熱暴露溫度升高,預(yù)形變表面形變組織呈現(xiàn)球化-零星不連續(xù)胞狀組織-連續(xù)胞狀組織-再結(jié)晶的動(dòng)態(tài)回復(fù)過程,硬化效果也隨之松弛;形變程度越大,在越低的溫度下開始出現(xiàn)動(dòng)態(tài)回復(fù)過程,但噴丸+1060℃/2h熱暴露并未觀察到再結(jié)晶。相比磨削狀態(tài),噴丸+熱暴露后1060℃軸向疲勞壽命有所提高。1060℃/350MPa/r=-1/軸向疲勞源呈現(xiàn)內(nèi)部萌生為主源,表面為次源的狀態(tài)。

    Abstract:

    [001] oriented DD11 single-crystal superalloy (SC) was shot-peened perpendicular to [001] to induce pre-deformation. Pre-deformed micro-structure was investigated using elecron backscatter diffraction (EBSD), scanning electron microscopy (SEM) and micro-hardness tester (HT). After subsequent thermal exposure (TE), the effect of the temperature and pre-deformation degree on surface structure was researched by SEM and HT, moreover, high-temperature fatigue performance after peening-exposure was tested. The results show that after pre-deformation, [110] and [111] oriented subgrains were observed on the surface, and that surface strain hardening effect occured. The greater the deformation degree was, the larger the subgrain orientation angle, the depth of the rotating subgrain layer and the hardening effect were. With the increase of exposure temperature, the pre-deformed surface micro-structure showed a relaxion of micro-hardness and a dynamic recovery process of spheroidization, fragmentation-discontinuous cellular organization and continuous cellular organization. Furthermore, the greater the deformation degree was, the lower temperature the recovery process occured at. However, the recrystallization was not observed at the condition of shot peening and 1060℃/2h. Compared with grinding and TE, the 1060℃ fatigue cycles increased while peening and TE. For fatigue condition 1060℃/350MPa/r=-1/axic, the main source of fatigue is sprouting inside, while secondary source is born on the surface.

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王 欣,艾瑩珺,湯智慧,劉晨光,李春志,趙振業(yè).熱暴露對表面預(yù)形變單晶合金組織和性能的影響[J].稀有金屬材料與工程,2019,48(2):573~579.[Wang Xin, Ai Yingjun, Tang Zhihui, Liu Chenguang, Zhao Zhenye, Li Chunzhi. Effect of Thermal Exposure on the Micro-structure and Performance of Surface Pre-deformed Single-crystal Superalloy[J]. Rare Metal Materials and Engineering,2019,48(2):573~579.]
DOI:10.12442/j. issn.1002-185X.20170598

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  • 收稿日期:2017-07-06
  • 最后修改日期:2017-08-26
  • 錄用日期:2017-09-12
  • 在線發(fā)布日期: 2019-03-15
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