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La-Ho-Fe合金的制備及其微波吸收特性研究
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材料科學與工程學院 桂林電子科技大學

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國家自然科學基金


Preparation and Microwave Absorption Propertiesof La-Ho-Fe Alloys
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School of Material Science and Engineering,Guilin University of Electronic Technology

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The National Natural Science Foundation of China

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    摘要:

    采用電弧熔煉及高能球磨工藝制備出LaxHo2-xFe17(x=0.0, 0.2, 0.4, 0.6, 0.8) 合金微粉,借助XRD、SEM、VSM和網(wǎng)絡(luò)矢量分析儀等儀器分別研究La替換對合金微粉的結(jié)構(gòu)、形貌、磁性能及其微波吸收性能的影響。結(jié)果表明, 隨著La含量的增加,飽和磁化強度和平均顆粒大小都有所增加。LaxHo2-xFe17合金的最小反射峰頻率向低頻方向移動。其中La0.2Ho1.8Fe17合金具有最好的吸波效果,在最佳匹配厚度1.8 mm下,La0.2Ho1.8Fe17合金的最小反射損耗在8.72 GHz處達到-28.72 dB,反射損耗小于-10 dB的頻帶寬度達到2.32 GHz。當厚度在1.2-2.4 mm范圍里,La0.2H1.8Fe17合金的反射損耗均小于-10 dB,這表明LaxHo2-xFe17是有前途的微波吸收材料,并具有良好的吸收特性。

    Abstract:

    The LaxHo2-xFe17 (x=0.0, 0.2, 0.4, 0.6, 0.8) powders were prepared by arc melting and high energy ball milling method. The influence of the La substitution on phase structure, morphology, magnetic properties and electromagnetic parameters were investigated by X-ray diffraction (XRD), scanning electron microscopy (SEM), vibrating-sample magnetometry (VSM) and vector network analyzer (VNA), respectively. The results show that the saturation magnetization increases and the average particle size increases with the increase of La content. The minimum absorption peak frequency shifts towards a lower frequency region with the increase of La content. The minimum RL of La0.2Ho1.8Fe17 reaches -28.72 dB at 8.72 GHz, and the frequency bandwidth of R<-10 dB reaches about 2.32 GHz with the best matching condition d=1.8 mm. The reflection loss with the thickness ranging of 1.2-2.4 mm could reach -10 dB, which indicates the particles be considered as the promising microwave absorbing materials with better absorption properties.

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羅家亮,潘順康,喬自強,成麗春,何煜,常鋆青. La-Ho-Fe合金的制備及其微波吸收特性研究[J].稀有金屬材料與工程,2018,47(12):3645~3650.[Luo Jialiang, Pan Shunkang, Qiao Ziqiang, Cheng Lichun, He Yu, Chang Junqing. Preparation and Microwave Absorption Propertiesof La-Ho-Fe Alloys[J]. Rare Metal Materials and Engineering,2018,47(12):3645~3650.]
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  • 收稿日期:2017-06-01
  • 最后修改日期:2017-08-26
  • 錄用日期:2017-09-12
  • 在線發(fā)布日期: 2019-01-04
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