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HPT不同壓力下純鉬組織性能及熱穩(wěn)定性研究
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作者單位:

合肥工業(yè)大學(xué) 材料科學(xué)與工程學(xué)院

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通訊作者:

中圖分類號(hào):

TG311

基金項(xiàng)目:

國(guó)家自然科學(xué)基金資助(項(xiàng)目號(hào)51675154),教育部新世紀(jì)優(yōu)秀人才支持計(jì)劃(2013JYXR0657)


Microstructure and Performance and Thermal Stability of Pure Molybdenum under Different Pressure by HPT
Author:
Affiliation:

Hefei University of Technology

Fund Project:

National Natural Science Foundation of China (51675154), New Century Excellent Talents in University (NCET-13-0765)

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    摘要:

    通過(guò)高壓扭轉(zhuǎn)實(shí)驗(yàn),在350℃條件下將難熔金屬純鉬粉末制備成相對(duì)密度達(dá)0.98以上的金屬鉬坯,利用多種檢測(cè)手段分析了高壓扭轉(zhuǎn)過(guò)程中鉬粉顆??紫堆葑兗爸旅軓?qiáng)化規(guī)律。通過(guò)改變預(yù)壓鉬坯壓力參數(shù),探討了壓力對(duì)壓扭鉬坯微觀結(jié)構(gòu)和力學(xué)性能及其熱穩(wěn)定性的影響。結(jié)果表明:壓力由2.0GPa增大到3.0GPa,壓扭鉬坯致密度提升顯著,其內(nèi)部亞晶尺寸細(xì)化,微觀應(yīng)變?cè)黾?試樣整體顯微硬度值隨壓力增大而升高,邊緣處略有降低。隨壓力增大,DSC后組織未發(fā)生顯著長(zhǎng)大,熱穩(wěn)定性較好。

    Abstract:

    The pure molybdenum powder was consolidated to bulk material with the relative density of over 0.98 via high-pressure torsion (HPT) processing at 350 ℃. The deformation of particles and pores, the evolution of crystallite size and dislocation density, and the strengthening mechanism during HPT processing were analyzed through scaning electron microscopy (SEM), X-ray diffraction (XRD) and the Vickers microhardness. The influence of applied pressure during HPT on the microstructure evolution, mechanical properties and thermal stability were discussed. The results show that the relative density and average microhardness of the HPT processed sample were improved obviously with the increasing applied pressure from 2.0 GPa to 3.0 GPa. Also, the crystallite size and microstrain experience a decrease and an increase with the increasing applied preassure which leads to the increase of dislocation density. In addition, the grain size in the HPT processed sample has a finite increase during the DSC processing, which indicates the thermal stability of HPT processed microstructure.

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李 萍,林 泉,聶愛(ài)琴,田 野,薛克敏. HPT不同壓力下純鉬組織性能及熱穩(wěn)定性研究[J].稀有金屬材料與工程,2019,48(2):673~677.[Ping Li, Quan Lin, Aiqin Nie, Ye Tian, Kemin Xue. Microstructure and Performance and Thermal Stability of Pure Molybdenum under Different Pressure by HPT[J]. Rare Metal Materials and Engineering,2019,48(2):673~677.]
DOI:10.12442/j. issn.1002-185X.20170458

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  • 收稿日期:2017-05-31
  • 最后修改日期:2017-06-16
  • 錄用日期:2017-06-26
  • 在線發(fā)布日期: 2019-03-15
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