41Sm5相,并促進(jìn)了Mg5Gd相析出。固溶時(shí)效處理后,晶界處粗大共晶組織溶解,析出相彌散分布,3%Sm的合金晶粒較細(xì)小,5%Sm的合金中出現(xiàn)短棒狀Mg5Gd相。在相同實(shí)驗(yàn)溫度下,隨著Sm含量的增加,合金的強(qiáng)度先升高后降低,3%Sm的合金抗拉強(qiáng)度最大。對(duì)于同一種合金,隨著拉伸溫度的升高抗拉強(qiáng)度先升高后降低,0~1% Sm的合金抗拉強(qiáng)度峰值出現(xiàn)在200℃,加入3~ 5%Sm的合金抗拉強(qiáng)度峰值出現(xiàn)在250℃??估瓘?qiáng)度具有明顯的反常溫度效應(yīng),而且Sm的加入強(qiáng)化了這種反常溫度效應(yīng)并使強(qiáng)度峰值出現(xiàn)的溫度升高。"/>

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Sm對(duì)Mg-10Gd-0.5Zr合金組織及力學(xué)性能的影響
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河南科技大學(xué) 材料科學(xué)與工程學(xué)院

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國(guó)家自然科學(xué)(51171059,51571084),河南省重點(diǎn)科技攻關(guān)項(xiàng)目(152102210072)。


Effect of Sm on microstructures and mechanical properties of Mg-10Gd-0.5Zr alloy
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School of Materials Science and Engineering,Henan University of Science and Technology

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    摘要:

    采用熔煉鑄造法制備了添加1-5wt%Sm的Mg-10Gd-0.5Zr合金,通過拉伸性能測(cè)試、掃描電鏡、X射線衍射分析研究了Sm對(duì)合金顯微組織和力學(xué)性能的影響。結(jié)果表明:Sm的加入形成了Mg41Sm5相,并促進(jìn)了Mg5Gd相析出。固溶時(shí)效處理后,晶界處粗大共晶組織溶解,析出相彌散分布,3%Sm的合金晶粒較細(xì)小,5%Sm的合金中出現(xiàn)短棒狀Mg5Gd相。在相同實(shí)驗(yàn)溫度下,隨著Sm含量的增加,合金的強(qiáng)度先升高后降低,3%Sm的合金抗拉強(qiáng)度最大。對(duì)于同一種合金,隨著拉伸溫度的升高抗拉強(qiáng)度先升高后降低,0~1% Sm的合金抗拉強(qiáng)度峰值出現(xiàn)在200℃,加入3~ 5%Sm的合金抗拉強(qiáng)度峰值出現(xiàn)在250℃??估瓘?qiáng)度具有明顯的反常溫度效應(yīng),而且Sm的加入強(qiáng)化了這種反常溫度效應(yīng)并使強(qiáng)度峰值出現(xiàn)的溫度升高。

    Abstract:

    Mg-10Gd-0.5Zr alloys with 1-5wt% Sm addition were prepared by melting and casting method. The effect of Sm on microstructures and mechanical properties were investigated by tensile tests, SEM and XRD. The results show that the Mg41Sm5 phase is found because of Sm addition, Sm promotes the precipitation of Mg5Gd. After solution-aging treatment, the coarsening eutectic structures at grain boundary were dissolved and the precipitation dispersed homogeneous. The finer grain size is observed when content of Sm come to 3wt%. Some of Mg5Gd phase become short rod-like when Sm addition is 5wt%. Under the same experimental temperature, the strength of tested alloys increases at fist and then decrease, and peak strength present when content of Sm is 3wt%. For the same alloy, with increasing of test temperature, the strength increase at fist and then decrease too. When Sm content is 0~1wt%, the temperature of tensile strength peak is 200℃ and the temperature is 250℃ when Sm content is 3~5wt%. There are abnormal temperature effects in tensile tests, the effect is reinforced and the temperature of tensile strength peak rise with the Sm addition.

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朱利敏,李全安,周耀,嚴(yán)景龍. Sm對(duì)Mg-10Gd-0.5Zr合金組織及力學(xué)性能的影響[J].稀有金屬材料與工程,2019,48(1):171~176.[Zhu Li-min, Li Quan-an, Zhou Yao, Yan Jing-long. Effect of Sm on microstructures and mechanical properties of Mg-10Gd-0.5Zr alloy[J]. Rare Metal Materials and Engineering,2019,48(1):171~176.]
DOI:10.12442/j. issn.1002-185X.20170425

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  • 收稿日期:2017-05-23
  • 最后修改日期:2017-09-19
  • 錄用日期:2017-10-12
  • 在線發(fā)布日期: 2019-02-18
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