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純度對ECAP制備超細(xì)晶銅疲勞性能的影響
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西安建筑科技大學(xué)冶金工程學(xué)院,西安建筑科技大學(xué)冶金工程學(xué)院,西安建筑科技大學(xué)冶金工程學(xué)院,西安建筑科技大學(xué)冶金工程學(xué)院

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國家自然科學(xué)基金資助(項(xiàng)目號(hào)51104113)


EFFECT OF PURITY ON FATIGUE PROPERTIES OF ULTRAFINE GRAINED CU PROCESSED BY EQUAL CHANNEL ANGULAR PRESSING
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School of Metallurgical and Engineering,Xi’an University of Architecture Technology,Xi’an 710055,School of Metallurgical and Engineering,Xi’an University of Architecture Technology,Xi’an 710055,School of Metallurgical and Engineering,Xi’an University of Architecture Technology,Xi’an 710055,School of Metallurgical and Engineering,Xi’an University of Architecture Technology,Xi’an 710055

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    摘要:

    等徑彎曲通道擠壓(ECAP)制備超細(xì)晶材料因具有優(yōu)異的機(jī)械性能而備受關(guān)注,其疲勞性能是獲得廣泛應(yīng)用的關(guān)鍵。本文采用應(yīng)力比R = -1的對稱加載疲勞試驗(yàn),研究了ECAP制備超細(xì)晶高純銅(LP Cu)、低純銅(HP Cu)的疲勞行為,分析了循環(huán)應(yīng)力-應(yīng)變響應(yīng)、疲勞壽命和疲勞前后晶粒取向分布,討論了純度與超細(xì)晶材料疲勞穩(wěn)定性的關(guān)系。結(jié)果表明:在任何應(yīng)力幅下,獲得的超細(xì)晶低純銅的壽命都大于ECAP變形前的粗晶銅,在相同應(yīng)力幅下,循環(huán)周次約提高到1.6~2.0倍。而超細(xì)晶高純銅的疲勞曲線,表現(xiàn)出不同的特性,在高應(yīng)力幅下,超細(xì)晶高純銅具有較高的疲勞壽命,但在低應(yīng)力幅下,超細(xì)晶高純銅循環(huán)周次下降,疲勞壽命低。在應(yīng)力控制條件下,隨應(yīng)力幅的降低,超細(xì)晶純銅的循環(huán)應(yīng)力-應(yīng)變響應(yīng)從循環(huán)軟化逐漸過渡為循環(huán)硬化。雜質(zhì)的存在能有效阻止疲勞過程晶粒的轉(zhuǎn)動(dòng)和位錯(cuò)的運(yùn)動(dòng),降低其回復(fù)軟化,減小相鄰晶粒間取向差變化,使超細(xì)晶低純銅與超細(xì)晶高純銅相比有較大的循環(huán)硬化指數(shù)n和循環(huán)硬化系數(shù)K,具有較好的疲勞穩(wěn)定性。

    Abstract:

    The ultra-fine grain(UFG) material by Equal Channel Angular Pressing (ECAP) has attracted attention for excellent mechanical performance. The fatigue properties of UFG by ECAPSareScriticalSto wide application. The fatigue properties of ultra-fine grain high purity(HP) and low purity(LP) copper by ECAP were investigated by fatigue tests conducted in air, at symmetrical loading ratio R= -1. The cyclic stress-strain response, fatigue life and grain orientation distribution before and after fatigue were analyzed. The relationship between purity and fatigue stability of ultra-fine grain copper were discussed. The results showed that the stress-controlled fatigue life of UFG low purity copper is longer about 1.6~2.0 times than that of their coarse grain (CG) counterparts under any stress amplitude. On the other hand, the fatigue curve of UFG high purity copper shows different characteristics. TheSfatigueScyclesSto failure of UFG Hp copper is strongly dependent upon the applied stress amplitude and decrease sharply withSstress amplitude decreasing. Under lower cyclic stresses, UFG Hp copper exhibitsSlower fatigue lives. Cyclic stress-strain response of UFG Cu under stress-controlled loading change from cyclic softening to cyclic hardening with stress amplitude decreasing. The UFG low purity copper shows a relatively high cyclic strain hardening exponent, hardeningShardeningScoefficient and fatigue stability with respect to the UFG high purity copper, because the impurity hinder grain rotation and dislocation motion, decline recovery rate, and reduce grain orientation modifies.

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王慶娟,周瀅,雙翼翔,杜忠澤.純度對ECAP制備超細(xì)晶銅疲勞性能的影響[J].稀有金屬材料與工程,2018,47(6):1806~1811.[WANG Qingjuan, ZHOU Ying, SUANG Yixiang, DU Zhongze. EFFECT OF PURITY ON FATIGUE PROPERTIES OF ULTRAFINE GRAINED CU PROCESSED BY EQUAL CHANNEL ANGULAR PRESSING[J]. Rare Metal Materials and Engineering,2018,47(6):1806~1811.]
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  • 收稿日期:2017-04-28
  • 最后修改日期:2017-06-22
  • 錄用日期:2017-06-23
  • 在線發(fā)布日期: 2018-09-06
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