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基于同步輻射CT技術(shù)表征3D打印用氣霧化TC4粉末的研究
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西北有色金屬研究院

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國家自然科學(xué)(51604228);陜西省科技統(tǒng)籌創(chuàng)新工程項(xiàng)目(2016KTZDCY-02-01)


Characterization of Gas-Atomized TC4 Powders for 3D Printing Based on Synchrotron Radiation CT Technique
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State Key Laboratory of Porous Metal Materials, Northwest Institute for Non-ferrous Metal Research

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    摘要:

    本研究利用氣霧化技術(shù)制備球形TC4合金粉末,作者利用SEM、同步輻射CT掃描-三維重建等分析手段對異常顆粒粉體以及不同粒徑的TC4合金粉末表面和內(nèi)部的孔缺陷進(jìn)行了表征。實(shí)驗(yàn)結(jié)果表明,本研究制備的TC4合金粉末隨著粉末粒徑減小,粉體表面由凸凹不平的冷凝收縮痕跡漸變?yōu)楣饣砻?粉體內(nèi)部的孔隙逐漸減少,且孔隙尺寸也隨之減??;經(jīng)分析,由于霧化過程中凝固與球化時(shí)間的差異及飛行軌跡的不同等原因?qū)е铝税?、連體式、橢球形、衛(wèi)星粉等異常粉末顆粒的生成;同步輻射CT掃描-三維重建表明,粉末內(nèi)部的孔隙率和孔隙尺寸隨著粉末粒度的增大而增大;作者認(rèn)為通過調(diào)整霧化工藝,使金屬熔滴在未開始冷卻凝固前徹底霧化破碎,從而能有效解決粉末內(nèi)部孔隙缺陷的問題。

    Abstract:

    In this study, spherical TC4 alloy powders were prepared by gas atomization. The surface and internal pore defects of TC4 alloy powders with different particle sizes were characterized by SEM, synchrotron radiation CT scanning and three-dimensional reconstruction. The experimental results show that the surface of the powder gradually changes from the condensed shrinkage trace to smooth surface with the decrease of particle size. The number and size of pores in powders also gradually decrease with decreasing the particle size. The formation of anomalous powders with the morphologies of wrapping, conjoined, ellipsoid and satellite is resulted from the difference of coagulation and spheroidization time and the different flight trajectories during the atomization process. The results of three-dimensional reconstruction by synchrotron radiation CT scanning show that the porosity and pore size of the powder increase with the increase of its particle size. The authors propose that if the metal droplet could be completely broken into tiny droplets during atomizing prior to its solidification by tailoring the atomizing parameters, internal porosity defects would be effectively minimized.

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趙少陽,湯慧萍,陳剛,殷京甌,王建,葛淵,李增峰,談萍.基于同步輻射CT技術(shù)表征3D打印用氣霧化TC4粉末的研究[J].稀有金屬材料與工程,2018,47(12):3853~3859.[Zhao Shaoyang, Tang Huiping, Chen Gang, Yin Jingou, Wang Jian, Ge Yuan, Li Zengfeng, Tan Ping. Characterization of Gas-Atomized TC4 Powders for 3D Printing Based on Synchrotron Radiation CT Technique[J]. Rare Metal Materials and Engineering,2018,47(12):3853~3859.]
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  • 收稿日期:2017-04-01
  • 最后修改日期:2017-05-31
  • 錄用日期:2017-06-23
  • 在線發(fā)布日期: 2019-01-04
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