2O3;攪拌摩擦加工;復(fù)合材料;組織;性能"/> 2O3含量的混合粉末(Ni+La2O3),制備 (Ni+La2O3)/Al復(fù)合材料。采用SEM、EDS、 EPMA及XRD對(duì)復(fù)合區(qū)微觀結(jié)構(gòu)及相組成進(jìn)行分析,采用室溫拉伸試驗(yàn)對(duì) (Ni+La2O3)/Al復(fù)合材料力學(xué)性能進(jìn)行了測(cè)試。結(jié)果表明,隨著La2O3含量的增加,(Ni+La2O3)/Al復(fù)合材料的組織和性能先變好后變差。當(dāng)La2O3添加量達(dá)到5%時(shí),復(fù)合材料中Al3Ni增強(qiáng)顆粒分布均勻、顆粒數(shù)量最多,塊狀的Ni粉團(tuán)聚減少,其抗拉強(qiáng)度達(dá)到最大值215MPa,相比Ni/Al復(fù)合材料(抗拉強(qiáng)度176MPa),其抗拉強(qiáng)度提高了22%;當(dāng)La2O3的添加量為7%時(shí),復(fù)合材料中Al3Ni增強(qiáng)顆粒含量減少,塊狀Ni粉團(tuán)聚重新出現(xiàn),抗拉強(qiáng)度下降至201MPa。"/>

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La2O3含量對(duì)攪拌摩擦加工制備Ni /Al復(fù)合材料組織和性能的影響
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西南昌航空大學(xué) 輕合金加工科學(xué)與技術(shù)國(guó)防重點(diǎn)學(xué)科實(shí)驗(yàn)室

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TB331

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國(guó)家自然科學(xué)基金(51465044, 51364037);江西省自然科學(xué)基金(20142BAB216019);江西省教育廳科技項(xiàng)目(GJJ160690)


Influence of La2O3 content on the microstructure and properties of Ni/Al composites fabricated by friction stir processing
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National Defence Key Discipline Laboratory of Light Alloy Processing Science and Techonology,Nachang Hangkong University

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    摘要:

    采用攪拌摩擦加工方法在Al基體中添加不同La2O3含量的混合粉末(Ni+La2O3),制備 (Ni+La2O3)/Al復(fù)合材料。采用SEM、EDS、 EPMA及XRD對(duì)復(fù)合區(qū)微觀結(jié)構(gòu)及相組成進(jìn)行分析,采用室溫拉伸試驗(yàn)對(duì) (Ni+La2O3)/Al復(fù)合材料力學(xué)性能進(jìn)行了測(cè)試。結(jié)果表明,隨著La2O3含量的增加,(Ni+La2O3)/Al復(fù)合材料的組織和性能先變好后變差。當(dāng)La2O3添加量達(dá)到5%時(shí),復(fù)合材料中Al3Ni增強(qiáng)顆粒分布均勻、顆粒數(shù)量最多,塊狀的Ni粉團(tuán)聚減少,其抗拉強(qiáng)度達(dá)到最大值215MPa,相比Ni/Al復(fù)合材料(抗拉強(qiáng)度176MPa),其抗拉強(qiáng)度提高了22%;當(dāng)La2O3的添加量為7%時(shí),復(fù)合材料中Al3Ni增強(qiáng)顆粒含量減少,塊狀Ni粉團(tuán)聚重新出現(xiàn),抗拉強(qiáng)度下降至201MPa。

    Abstract:

    : (Ni+La2O3)/Al composites were fabricated by means of adding the mixed powder of (Ni+La2O3) with different La2O3 content to the Al substrate in the Friction Stir Processing (FSP) period. The microstructures of the composite zone were analyzed by SEM and EDS, the element distribution of the composite zone were analyzed by EPMA, the phase composition was examined by XRD, the mechanical properties of the composites were tested by tensile test at room temperature. Results show that: The microstructure and properties of (Ni+La2O3)/Al composites trend to be better firstly and then worse with increasing of La2O3 contents. When the contents of La2O3 are 5%, the contents of Al3Ni particles increase and the distribution of particles becomes uniform,the massive Ni agglomerates are decreased, so the tensile strength of the composites is the highest with 215MPa, which is increased by 22% than that of Ni/Al composites(The tensile strength is 176MPa); When the contents of La2O3 are 7%, the contents of Al3Ni particles decrease and the massive Ni agglomerates reappear, the tensile strength of the composites decreased to 201MPa.

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汪云海,夏 春,黃春平,劉奮成,柯黎明. La2O3含量對(duì)攪拌摩擦加工制備Ni /Al復(fù)合材料組織和性能的影響[J].稀有金屬材料與工程,2018,47(12):3829~3834.[Wang Yunhai, Xia Chun, Huang Chunping, Liu Fencheng, Ke Liming. Influence of La2O3 content on the microstructure and properties of Ni/Al composites fabricated by friction stir processing[J]. Rare Metal Materials and Engineering,2018,47(12):3829~3834.]
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  • 收稿日期:2017-03-21
  • 最后修改日期:2017-09-11
  • 錄用日期:2017-09-29
  • 在線發(fā)布日期: 2019-01-04
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