-4-1.32×10-2 s-1條件下的高溫拉伸變形試驗(yàn)研究,利用電子背散射技術(shù)(EBSD)表征了不同變形條件下的晶粒形貌、晶粒取向和分布規(guī)律。結(jié)果表明:TA32合金具有良好的超塑性變形能力,最大斷裂延伸率能達(dá)到1141.8%。在高溫和低應(yīng)變速率條件下,晶粒的長大容易造成在變形后期真實(shí)應(yīng)力出現(xiàn)上升現(xiàn)象。真實(shí)應(yīng)力和斷裂延伸率對變形溫度、變形程度和應(yīng)變速率均是敏感的,動態(tài)再結(jié)晶容易在高溫或低應(yīng)變速率條件下發(fā)生。動態(tài)再結(jié)晶程度隨著變形溫度的升高、應(yīng)變速率的降低和變形程度的增大而增大,變形后的織構(gòu)接近隨機(jī)取向織構(gòu),原始晶粒得到等軸化,提高了晶粒尺寸的均勻性。在變形過程中,不連續(xù)動態(tài)再接晶是主要的動態(tài)再結(jié)晶機(jī)制,隨著變形溫度的升高、應(yīng)變速率的降低和變形程度的增大,不連續(xù)動態(tài)再結(jié)晶的作用在增強(qiáng),連續(xù)動態(tài)再結(jié)晶的作用則是在減弱。"/>

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變形參數(shù)對TA32合金的超塑性變形行為及微觀組織演化的影響
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作者單位:

1.清華大學(xué)機(jī)械工程系;2.北京星航機(jī)電裝備有限公司

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中圖分類號:

TG146.2

基金項(xiàng)目:

國家自然科學(xué)基金資助(51471090)


Effects of deformation parameters on the microstructure evolution and superplastic behavior of TA32 alloy
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Affiliation:

1.Department of Mechanical Engineering,Tsinghua University;2.Beijing Xinghang Electro-mechanical Equipment Co,Ltd

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    針對我國自主研制的TA32高溫鈦合金,開展了在變形溫度為895-935℃和應(yīng)變速率為8.3×10-4-1.32×10-2 s-1條件下的高溫拉伸變形試驗(yàn)研究,利用電子背散射技術(shù)(EBSD)表征了不同變形條件下的晶粒形貌、晶粒取向和分布規(guī)律。結(jié)果表明:TA32合金具有良好的超塑性變形能力,最大斷裂延伸率能達(dá)到1141.8%。在高溫和低應(yīng)變速率條件下,晶粒的長大容易造成在變形后期真實(shí)應(yīng)力出現(xiàn)上升現(xiàn)象。真實(shí)應(yīng)力和斷裂延伸率對變形溫度、變形程度和應(yīng)變速率均是敏感的,動態(tài)再結(jié)晶容易在高溫或低應(yīng)變速率條件下發(fā)生。動態(tài)再結(jié)晶程度隨著變形溫度的升高、應(yīng)變速率的降低和變形程度的增大而增大,變形后的織構(gòu)接近隨機(jī)取向織構(gòu),原始晶粒得到等軸化,提高了晶粒尺寸的均勻性。在變形過程中,不連續(xù)動態(tài)再接晶是主要的動態(tài)再結(jié)晶機(jī)制,隨著變形溫度的升高、應(yīng)變速率的降低和變形程度的增大,不連續(xù)動態(tài)再結(jié)晶的作用在增強(qiáng),連續(xù)動態(tài)再結(jié)晶的作用則是在減弱。

    Abstract:

    High-temperature tensile test at a deformation temperature of 895-935℃ and a strain rate of 8.3×10-4-1.32×10-2 s-1 is conducted for TA32 high-temperature titanium alloy developed independently by our country, and electron back-scattered diffraction (EBSD) technique is used to characterize grain morphology, orientation, and grain distribution. The results show that TA32 alloy provides superior superplastic deformation capability, with a maximum fracture elongation up to 1141.8%. In high temperature and low strain rate conditions, growth of grains tends to result in the rise of true stress in late deformation stages. Both the true stress and fracture elongation are sensitive to deformation temperature, deformation degree, and strain rate. Dynamic recrystallization is more likely to occur in high temperature or low strain rate conditions. The degree of dynamic recrystallization increases with the increasing deformation temperature, the decrease of strain rate, or the increase of deformation degree. After deformation, the textures nearly exhibit random orientations, and the original grains get equiaxed with better dimensional uniformity. During the process of deformation, discontinuous dynamic recrystallization serves as the dominant dynamic recrystallization mechanism. With the increase of deformation temperature, decrease of strain rate, or increase of deformation degree, discontinuous dynamic recrystallization plays a more important role, while continuous dynamic recrystallization weakens.

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劉章光,李培杰,尹西岳,仵鳳勇,熊亮同,高海濤.變形參數(shù)對TA32合金的超塑性變形行為及微觀組織演化的影響[J].稀有金屬材料與工程,2018,47(11):3473~3481.[Liu Zhangguang, Li Peijie, Yin Xiyue, Wu Fengyong, Xiong Liangtong, Gao Haitao. Effects of deformation parameters on the microstructure evolution and superplastic behavior of TA32 alloy[J]. Rare Metal Materials and Engineering,2018,47(11):3473~3481.]
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  • 收稿日期:2017-03-16
  • 最后修改日期:2017-04-04
  • 錄用日期:2017-04-14
  • 在線發(fā)布日期: 2018-12-19
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