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時效處理對20%冷變形15Cr-15Ni含Ti奧氏體不銹鋼組織和高溫力學性能的影響
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1.中國科學院核用材料與安全評價重點實驗室中國科學院金屬研究所;2.中國原子能科學研究院

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Influence of Aging Treatment on the Microstructure and High Temperature Mechanical Properties for 15Cr-15Ni Titanium-modified Austenitic Stainless Steel in 20% Cold-worked Condition
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    摘要:

    針對鈉冷快堆包殼管用15Cr-15Ni含Ti的奧氏體不銹鋼,研究了550-750℃時效處理336h對20%冷變形合金組織和650℃拉伸性能的影響。結果表明:在550℃時效336h后,合金發(fā)生回復,組織中位錯移動產生大量退火孿晶。當在650℃和750℃時效時,合金進一步回復,孿晶數量明顯減少,且在組織中發(fā)現有Sigma相析出。隨時效溫度的升高,sigma相數量和尺寸增加。與20%冷變形合金650℃拉伸性能相比,550℃時效態(tài)樣品拉伸時,合金屈服和抗拉強度略有增加;隨著時效溫度的升高,合金屈服和抗拉強度顯著降低。與拉伸強度相比,時效態(tài)合金的延伸率變化趨勢與之相反,時效溫度升高,合金的延伸率提高。

    Abstract:

    Titanium-stabilized 15Cr-15Ni austenitic stainless steel in 20% cold-worked condition has been considered as a promising candidate high temperature structural material for core components in liquid metal-cooled fast reactors (LMFR). Microstructure and high temperature mechanical properties of as cold-worked and different aging treatments alloys were investigated by using metallographic microscope, scanning and transmission electron microscope, and tensile testing machine. The results demonstrate that the recovery took place when the alloys were aged at 550℃ for 336h. The emergence abundant of twins was attributed to dislocations movement. When aging temperature increasing to 650℃ and 750℃, the amount of twins reduced because of alloy′s further recover. Sigma phase precipitated from austenitic matrix along grain boundaries when alloys were aged at 650-750℃ for 336h. The amount and size of sigma phase increased with the aging temperature and time increasing. Because of the grain boundary strengthening, alloys aged at 550℃ had slightly higher yield strength and ultimate tensile strength than those of as-cold worked alloy. The high temperature yield strength and ultimate tensile strength decreased significantly, while plasticity increased observably when aging temperature increasing to 650℃ and 750℃.

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王志楠,梁田,張龍,杜愛兵,高明,馬穎澈,劉奎.時效處理對20%冷變形15Cr-15Ni含Ti奧氏體不銹鋼組織和高溫力學性能的影響[J].稀有金屬材料與工程,2018,47(11):3504~3511.[wangzhinan, Liang Tian, zhang Long, Du Aibing, Gao Ming, Ma Yingche, Liu Kui. Influence of Aging Treatment on the Microstructure and High Temperature Mechanical Properties for 15Cr-15Ni Titanium-modified Austenitic Stainless Steel in 20% Cold-worked Condition[J]. Rare Metal Materials and Engineering,2018,47(11):3504~3511.]
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  • 收稿日期:2017-02-13
  • 最后修改日期:2017-04-25
  • 錄用日期:2017-05-16
  • 在線發(fā)布日期: 2018-12-19
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