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一種鎳基單晶高溫合金870℃高周疲勞變形微觀結(jié)構(gòu)研究
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沈陽理工大學(xué)

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TG132.3

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國家自然科學(xué)基金項(xiàng)目(面上項(xiàng)目,重點(diǎn)項(xiàng)目,重大項(xiàng)目)


Study of Dislocation Structure in a Single Crystal Nickel Base Duiring High Cycle Fatigue
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    摘要:

    摘 要:本文研究了一種鎳基單晶高溫合金在870℃℃時(shí)的高周疲勞性能及其變形組織結(jié)構(gòu)。結(jié)果表明:該合金的疲勞壽命隨著應(yīng)力水平的升高而減小,870℃℃時(shí)光滑試樣的疲勞強(qiáng)度為443MPa;利用透射電鏡(TEM)觀察疲勞循環(huán)試樣的位錯(cuò)組態(tài),發(fā)現(xiàn)在疲勞變形的初始和中期階段,位錯(cuò)組態(tài)主要為界面位錯(cuò),位錯(cuò)在基體通道中{111}面運(yùn)動(dòng),并交互反應(yīng)形成3維位錯(cuò)網(wǎng)絡(luò)結(jié)構(gòu)。當(dāng)應(yīng)力水平提高到550MPa以上時(shí),在變形的末期,觀察到高密度位錯(cuò)集中于位錯(cuò)滑移帶及位錯(cuò)切入??r" 相現(xiàn)象。在循環(huán)應(yīng)力和高溫疊加作用下,基體通道中誘發(fā)析出大量圓形細(xì)小二次?r’? 相。二次?r"?相的析出有益于阻止基體位錯(cuò)的滑動(dòng),抑制位錯(cuò)切入?r"?相,有利于提高合金的疲勞強(qiáng)度。

    Abstract:

    Abstract: An investigation of dislocation structure and its impact on the mechanical behavior of a ?? strengthened nickel base single crystal alloy under high cycle fatigue (HCF) at 870℃ is studied. The results indicate that HCF lifetime reduced with increase of applied stress amplitude. In the early stages, the fatigue deformation occurs by forced bowing of dislocations through the narrow ? matrix channels on {111} planes. During mid-term fatigue stages, most of the dislocations formed in the matrix are located in the r?/ r"?? interfaces, their intersection and reaction produce new dislocation segments and three-dimensional dislocation networks. The Burgers vectors of the dislocations in the network are 1/2<110>. The interaction of cyclic stress with high temperature induced the precipitation of homogeneous globular r"?? precipitates, that is beneficial to fatigue strength. At the end of fatigue test, the cyclic stress led to the formation of persistent slip bands moving through the r? matrix channels and ?r‘? particles. Dislocation shearing through the r"?? phase was found occasionally. The extrinsic stacking faults was also observed in the present study.

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水麗.一種鎳基單晶高溫合金870℃高周疲勞變形微觀結(jié)構(gòu)研究[J].稀有金屬材料與工程,2018,47(4):1054~1058.[Sui LI. Study of Dislocation Structure in a Single Crystal Nickel Base Duiring High Cycle Fatigue[J]. Rare Metal Materials and Engineering,2018,47(4):1054~1058.]
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  • 收稿日期:2016-09-27
  • 最后修改日期:2018-04-19
  • 錄用日期:2016-12-02
  • 在線發(fā)布日期: 2018-05-31
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