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基材溫度對采用磁控濺射制備的Ti-Al-Si-Cu-N涂層的微觀結構及摩擦學性能的影響
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南昌航空大學,南昌航空大學

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國家自然科學基金項目(面上項目,重點項目,重大項目)


Effects of substrate temperature on microstructure and tribological properties of Ti-Al-Si-Cu-N films deposited by magnetron sputtering
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Nanchang Hangkong University,Nanchang Hangkong University

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    摘要:

    本文中,采用反應磁控濺射技術在304不銹鋼基片上沉積Ti-Al-Si-Cu-N涂層。通過掃描電鏡(SEM)、能譜儀(EDS)、X射線衍射儀(XRD)、納米壓痕儀、劃痕儀和球盤式摩擦磨損試驗機研究了不同的基材溫度對涂層結構和摩擦學性能的影響。結果表明:隨著沉積溫度從室溫升至250 oC,涂層變得表面平滑,結構致密。硬度和彈性模量隨沉積溫度的升高而升高。劃痕實驗表明:當沉積溫度分別為室溫,150 oC 和250 oC時,臨界載荷為3.85 N, 3.45 N 和5.10 N。當沉積溫度為250 oC時,涂層的摩擦系數(shù)和磨損量最小,磨損機制主要為磨粒磨損摩擦過程中產(chǎn)生的磨屑主要來自GCr15不銹鋼珠。在較低的沉積溫度下,涂層的磨損機理主要為脆性斷裂和磨粒磨損。

    Abstract:

    In this study, Ti-Al-Si-Cu-N films were deposited on the AISI-304 stainless steel by reactive magnetron sputtering technology. The influences of the substrate temperature on the microstructure and properties of the films were researched by scanning electron microscope(SEM),energy disperse spectroscopy(EDS), X-ray diffraction (XRD), a nano-indenter, a scratch tester and a ball-on-disc rotational tribometer. The results indicated that when the deposition temperature increased from room temperature to 250 oC, the films became smoother and denser. The hardness and elastic modulus increased with the increase of the deposition temperature. The scratch test showed that when the deposition temperatures were RT, 150 oC and 250 oC, the critical load of the films was 3.85 N, 3.45 N and 5.10 N, respectively. The friction coefficient and wear rate of the Ti-Al-Si-Cu-N film deposited at 250 oC were the smallest, and the wear debris was mainly from the counterparts GCr15 stainless balls, the wear mechanism of the films deposited at lower temperatures was mainly fatigue fracture and abrasive wear, while that of the film deposited at 250 oC was abrasive wear.

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馮長杰,陳恩.基材溫度對采用磁控濺射制備的Ti-Al-Si-Cu-N涂層的微觀結構及摩擦學性能的影響[J].稀有金屬材料與工程,2017,46(6):1497~1502.[fengchangjie, chenen. Effects of substrate temperature on microstructure and tribological properties of Ti-Al-Si-Cu-N films deposited by magnetron sputtering[J]. Rare Metal Materials and Engineering,2017,46(6):1497~1502.]
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  • 收稿日期:2016-06-14
  • 最后修改日期:2016-09-15
  • 錄用日期:2016-10-18
  • 在線發(fā)布日期: 2017-11-07
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