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稀土金屬提純方法與研究進(jìn)展
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北京大學(xué),全球能源互聯(lián)網(wǎng)研究院 先進(jìn)輸電技術(shù)國家重點(diǎn)實(shí)驗(yàn)室電工新材料技術(shù)聯(lián)合實(shí)驗(yàn)室,北京大學(xué)化學(xué)與分子工程學(xué)院,北京大學(xué)化學(xué)與分子工程學(xué)院

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TF845

基金項(xiàng)目:

國家重點(diǎn)基礎(chǔ)研究發(fā)展計劃(973計劃) (2012CBA01207) 、國家自然科學(xué)基金委項(xiàng)目(No. U1201241, 11375020, 51431001)


Research progress and technology of rare earth metal purification
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Peking University,Global Energy Interconnection Research institute,State Key laboratory of Advanced Transmission Technology,Material Laboratory of State Grid Corporation of China,Beijing,College of Chemistry and Molecular Engineering,Peking University,Beijing,College of Chemistry and Molecular Engineering,Peking University,Beijing

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    摘要:

    隨著稀土材料不斷開發(fā),新型稀土功能材料的制備需要純度更高的稀土金屬,稀土金屬提純方法包括真空熔煉、電解精煉、真空蒸餾/升華、熔鹽萃取、區(qū)域熔煉、固態(tài)電遷移、電化學(xué)脫氧、外吸氣劑法、 通氫等離子體熔煉等。本文對各種方法提純稀土金屬的機(jī)理進(jìn)行了闡述,對研究現(xiàn)狀和提純效果進(jìn)行了總結(jié)。雜質(zhì)去除需采用多種手段結(jié)合,同時提升裝備水平,以達(dá)到提高提純效果、降低成本、縮短生產(chǎn)周期的目的。

    Abstract:

    Along with the development of rare earth materials, the preparation of novel rare earth function materials needed higher purity of rare earth metals. The methods for purifying rare earth metal mainly included vacuum melting, electrolytic refining, vacuum distillation/sublimation, fused-salt extraction, zone refining, solid-state electrotransport, electrochemical deoxidation, external getter method, plasma arc melting (Ar or Ar+H2), etc. The purification mechanism of rare earths metals was briefly explained, and the research progress and purification effects are summarized. Combining multiple means for removing impurities and promoting the level of equipment, in order to improve the effects of purification, and reduce the cost, shorten production cycle.

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李吉剛,徐麗,李國玲,李星國.稀土金屬提純方法與研究進(jìn)展[J].稀有金屬材料與工程,2018,47(5):1648~1654.[Li Jigang, Xu Li, Li Guoling, Li Xingguo. Research progress and technology of rare earth metal purification[J]. Rare Metal Materials and Engineering,2018,47(5):1648~1654.]
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  • 收稿日期:2016-05-10
  • 最后修改日期:2016-07-12
  • 錄用日期:2016-08-17
  • 在線發(fā)布日期: 2018-06-08
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