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PREP法制備Ti-60Ta合金粉末及其性能研究
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西北有色金屬研究院,西北有色金屬研究院,西北有色金屬研究院,西北有色金屬研究院

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陜西省科技統(tǒng)籌創(chuàng)新工程計(jì)劃項(xiàng)目(2016KTCQ01-113);陜西省青年科技新星項(xiàng)目(2016KJXX-78);獲中南大學(xué)粉末冶金國家重點(diǎn)實(shí)驗(yàn)室資助


An investigation of Ti-60Ta powders produced by PREP
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    摘要:

    本研究利用等離子旋轉(zhuǎn)電極霧化技術(shù)制備出球形Ti-60Ta合金粉末,作者利用SEM、XRD和維氏顯微硬度測(cè)試儀等分析手段對(duì)不同粒徑的Ti-60Ta合金粉末表面及內(nèi)部的顯微形貌、相組成、樹枝晶間距和維氏顯微硬度進(jìn)行了表征。實(shí)驗(yàn)結(jié)果表明,本研究制備的Ti-60Ta合金粉末主要以β相為主,細(xì)粒徑粉末還有少量馬氏體α"相和ω相;大顆粒粉末的表面呈近似等軸花瓣?duì)畹臉渲ЫM織,小顆粒粉末表面枝晶組織則明顯細(xì)化,并觀察到細(xì)針狀馬氏體;隨著粉末粒度減小,馬氏體相增多,維氏顯微硬度逐漸增大。

    Abstract:

    In this study, Ti-60Ta powders were produced by the plasma rotating electrode processing technique. The surface and internal microstructural morphologies, phase compositions, distances between dendrites and micro-hardness have been characterized for powders with different size ranges by SEM、XRD and Vickers micro-hardness methods. Results showed that the prepared Ti-60Ta powders exhibited major β phase and a small amount of martensitic α" and ω phases; the surface of larger particles appears isometric petal-shaped dentritic microstructures, while small particles exhibit refined dendritic microstructures. Particularly, fine acicular martensitic appearance was observed on the smaller particles. As the powder particle size decreases, the martensite phases increase and accordingly Vickers micro-hardness increases.

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趙少陽,殷京甌,沈 壘,陳 剛. PREP法制備Ti-60Ta合金粉末及其性能研究[J].稀有金屬材料與工程,2017,46(6):1679~1683.[Zhao Shaoyang, Yin Jingou, Shen Lei, Chen Gang. An investigation of Ti-60Ta powders produced by PREP[J]. Rare Metal Materials and Engineering,2017,46(6):1679~1683.]
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  • 收稿日期:2016-04-30
  • 最后修改日期:2016-07-15
  • 錄用日期:2016-08-17
  • 在線發(fā)布日期: 2017-11-07
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