on(占空比)可以獲得較大峰值電流,并對薄膜的微觀結(jié)構(gòu)產(chǎn)生顯著影響。薄膜的表面生長形貌表現(xiàn)為隨著單脈沖持續(xù)時間的延長,顆粒間逐漸出現(xiàn)明顯的孔隙,圓球狀團(tuán)聚生長的尺寸明顯增大。截面生長形貌表現(xiàn)為隨著脈沖持續(xù)時間的延長,發(fā)生由柱狀形貌向樹枝狀形貌過渡,并產(chǎn)生大量的孔隙與缺陷,薄膜致密度明顯下降。力學(xué)性能表現(xiàn)為隨著脈沖持續(xù)時間的延長,薄膜的硬度與模量都呈現(xiàn)出先增大后大幅降低的變化趨勢,且當(dāng)單脈沖持續(xù)時間為4ms左右時,薄膜的硬度與模量存在最大值。"/>

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脈沖持續(xù)時間對Ti納米晶薄膜結(jié)構(gòu)及性能的影響
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西安理工大學(xué)材料科學(xué)與工程學(xué)院,西安理工大學(xué)材料科學(xué)與工程學(xué)院,南昌大學(xué)材料科學(xué)與工程學(xué)院材料科學(xué)研究所,西安市碑林區(qū)金花南路5號西安理工大學(xué)材料科學(xué)與工程學(xué)院

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TB303

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國家自然科學(xué)基金資助(項目號52171144)


Effect of pulse duration on the structure and properties of Ti nano-crystalline films
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xi''an university of technology,,,

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    摘要:

    采用大功率脈沖離子鍍技術(shù),通過調(diào)控單脈沖持續(xù)時間的方式,對所制備的純金屬細(xì)晶粒Ti薄膜的微觀結(jié)構(gòu)以及相關(guān)力學(xué)性能進(jìn)行了對比研究。結(jié)果表明:在較小平均電流條件下,通過調(diào)控脈單沖持續(xù)時間Ton(占空比)可以獲得較大峰值電流,并對薄膜的微觀結(jié)構(gòu)產(chǎn)生顯著影響。薄膜的表面生長形貌表現(xiàn)為隨著單脈沖持續(xù)時間的延長,顆粒間逐漸出現(xiàn)明顯的孔隙,圓球狀團(tuán)聚生長的尺寸明顯增大。截面生長形貌表現(xiàn)為隨著脈沖持續(xù)時間的延長,發(fā)生由柱狀形貌向樹枝狀形貌過渡,并產(chǎn)生大量的孔隙與缺陷,薄膜致密度明顯下降。力學(xué)性能表現(xiàn)為隨著脈沖持續(xù)時間的延長,薄膜的硬度與模量都呈現(xiàn)出先增大后大幅降低的變化趨勢,且當(dāng)單脈沖持續(xù)時間為4ms左右時,薄膜的硬度與模量存在最大值。

    Abstract:

    The microstructure and mechanical properties of nano-crystalline Ti films were studied with different pulse duration,which were deposited by the High Power Pulsed ion plating. The results shows that when the average current kept in low value, the larger peak current can be obtained by adjusting the pulse duration (duty ratio), which has a significant effect on the microstructure of the thin film. The surface morphologies showed gradually appeared apparent porosity of the particles and the growth dimensions of the spherical agglomeration significantly increases with the single pulses duration prolonged. The cross section of the growth showed that the morphology transition from the columnar to the dendritic with the extension of the duration of the pulse, while a large number of pores and defects occurred and the density of the films decreased obviously. The hardness and modulus of the films are showing increased first and the substantially reduced trend with the prolonged of the pulse duration. The value of the hardness and modulus exist the maximum when the single pulse duration reached about 4ms.

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喬泳彭,蔣百靈.,曹政,張冰.脈沖持續(xù)時間對Ti納米晶薄膜結(jié)構(gòu)及性能的影響[J].稀有金屬材料與工程,2018,47(5):1596~1600.[Qiao Yongpeng, Jiang Bailing, Cao Zheng, Zhang bing. Effect of pulse duration on the structure and properties of Ti nano-crystalline films[J]. Rare Metal Materials and Engineering,2018,47(5):1596~1600.]
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  • 收稿日期:2016-04-25
  • 最后修改日期:2016-07-14
  • 錄用日期:2016-08-17
  • 在線發(fā)布日期: 2018-06-08
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