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真空氣壓浸滲3D-Cf/Al復(fù)合材料微觀缺陷分析
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1.南昌航空大學(xué) 輕合金加工科學(xué)與技術(shù)國防重點學(xué)科實驗室,1.南昌航空大學(xué) 輕合金加工科學(xué)與技術(shù)國防重點學(xué)科實驗室,1.南昌航空大學(xué) 輕合金加工科學(xué)與技術(shù)國防重點學(xué)科實驗室,1.南昌航空大學(xué) 輕合金加工科學(xué)與技術(shù)國防重點學(xué)科實驗室,1.南昌航空大學(xué) 輕合金加工科學(xué)與技術(shù)國防重點學(xué)科實驗室

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TB331

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國家自然科學(xué)基金資助項目(51365043);江西省自然科學(xué)基金資助項目(20151BAB206004);輕合金加工科學(xué)與技術(shù)國防重點學(xué)科實驗室和航空材料熱加工技術(shù)航空科技重點實驗室聯(lián)合資助項目(GF201101004)


Micro defects analysis of 3D-Cf/Al composites by vacuum pressure infiltration
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National Defence Key Discipline Laboratory of Light Alloy Processing Science and Technology,Nanchang Hangkong University,National Defence Key Discipline Laboratory of Light Alloy Processing Science and Technology,Nanchang Hangkong University,National Defence Key Discipline Laboratory of Light Alloy Processing Science and Technology,Nanchang Hangkong University,National Defence Key Discipline Laboratory of Light Alloy Processing Science and Technology,Nanchang Hangkong University,National Defence Key Discipline Laboratory of Light Alloy Processing Science and Technology,Nanchang Hangkong University

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    摘要:

    采用真空氣壓浸滲法制備了纖維體積分數(shù)51%、致密度≥97%的三維五向和三維正交編織M40碳纖維增強鋁基復(fù)合材料(3D-Cf/Al),分析了復(fù)合材料中微觀缺陷的形貌、形成機理及其控制手段,并對比了兩種編織結(jié)構(gòu)對復(fù)合材料微觀缺陷形成的影響。結(jié)果表明:復(fù)合材料中的缺陷均是微米級的微觀缺陷,主要有束內(nèi)孔隙、局部纖維偏聚及在基體集聚處的冷隔、顯微縮孔及微夾雜等,其中三維正交Cf/Al復(fù)合材料束內(nèi)孔隙及束間孔隙較三維五向Cf/Al復(fù)合材料少,而局部纖維偏聚現(xiàn)象較三維五向Cf/Al復(fù)合材料嚴重,造成其缺陷差異的主要原因在于其纖維預(yù)制體編織結(jié)構(gòu)的差異,通過提高預(yù)熱溫度可以顯著減少復(fù)合材料內(nèi)部的孔隙缺陷及局部纖維偏聚現(xiàn)象。

    Abstract:

    The vacuum gas pressure infiltration was performed by 3D five-directional and 3D orthogonal braided performs woven by M40 graphite fiber composite (3D-Cf/Al) with the volume fraction of 51% and the density higher than 97%. After analyzing the morphology and formation mechanism of micro defects and control measures, and comparing the effects of braiding structures on micro defect formation, the results showed that the defects in the composite were micron grade micro defects, of which the main defects included pores within the fiber beam and partial fiber reunited, cold shut, microscopy shrinkage cavity and small inclusion in the substrate concentration. Of note the pores between the fiber beam and pores within the fiber beam of 3D orthogonal composite were less than 3D five-directional composite, while the fiber reunited phenomenon of 3D orthogonal composite was more serious than 3D five-directional composite. The main reason for the different defects was braided structure distinctions. By increasing the fiber preheat temperature could effectively reduce the internal pores defect and partial fiber reunited phenomenon.

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聶明明,徐志鋒,余歡,王振軍,蔡長春.真空氣壓浸滲3D-Cf/Al復(fù)合材料微觀缺陷分析[J].稀有金屬材料與工程,2018,47(4):1266~1274.[Nie Mingming, Xu Zhifeng, Yu Huan, Wang Zhenjun, Cai Changchun. Micro defects analysis of 3D-Cf/Al composites by vacuum pressure infiltration[J]. Rare Metal Materials and Engineering,2018,47(4):1266~1274.]
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  • 收稿日期:2016-03-14
  • 最后修改日期:2016-07-05
  • 錄用日期:2016-08-17
  • 在線發(fā)布日期: 2018-05-31
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