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磁控濺射法制備碳/碳復(fù)合材料 SiC/MoSi2-ZrB2 涂層的結(jié)構(gòu)及抗氧化性能研究
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中南大學(xué)材料科學(xué)與工程學(xué)院, 廣東省新材料研究所,廣東省新材料研究所,廣東省新材料研究所,廣東省新材料研究所,廣東省新材料研究所

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廣東省金屬材料與加工專業(yè)鎮(zhèn)聯(lián)合創(chuàng)新公共平臺(tái)


Microstructure and Anti-oxidation Properties of SiC/MoSi2-ZrB2 Coating for Carbon/ Carbon Composites Prepared by Magnetron Sputtering
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    摘要:

    通過(guò)磁控濺射法在碳/碳復(fù)合材料表面成功制得了SiC/MoSi2-ZrB2陶瓷涂層并對(duì)結(jié)構(gòu)及其在高溫有氧環(huán)境中的抗氧化性能進(jìn)行了研究。結(jié)果表明制備的SiC/MoSi2-ZrB2陶瓷涂層呈柱狀晶結(jié)構(gòu)且均勻性良好,其在1273K和1773K的有氧環(huán)境中氧化60min失重率分別是5.6×10-2 g/cm2 和 6.3×10-2 g/cm2。

    Abstract:

    A SiC/MoSi2-ZrB2 ceramic coating was prepared by a magnetron sputtering method on carbon/carbon composites to protect it against oxidation. The microstructure of the coating was investigated, and its oxidation behavior at 1273K and 1773 K in air was also studied. The as-received coating exhibited outstanding uniformity in thickness and presented columnar structure. The coated C/C composites performed a superior oxidation resistance, and the weight loss of the samples after oxidation at 1273K and 1773 K for 60min in oxygen containing environment was 5.6×10-2 g/cm2 and 6.3×10-2 g/cm2 , respectively.

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楊艷姣,代明江,韋春貝,侯慧君,林松盛.磁控濺射法制備碳/碳復(fù)合材料 SiC/MoSi2-ZrB2 涂層的結(jié)構(gòu)及抗氧化性能研究[J].稀有金屬材料與工程,2017,46(12):3663~3668.[Yang Yanjiao, Dai Mingjiang, Wei Chunbei, Hou Huijun, Ling Songsheng. Microstructure and Anti-oxidation Properties of SiC/MoSi2-ZrB2 Coating for Carbon/ Carbon Composites Prepared by Magnetron Sputtering[J]. Rare Metal Materials and Engineering,2017,46(12):3663~3668.]
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  • 收稿日期:2016-01-15
  • 最后修改日期:2016-04-08
  • 錄用日期:2016-04-26
  • 在線發(fā)布日期: 2018-01-04
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