f/Al復合材料;微觀組織;界面;力學性能;高溫"/> f/Al復合材料,研究了不同溫度制備的復合材料微觀組織特征和界面反應程度,測試了復合材料在室溫和高溫下的拉伸力學性能并分析了其斷口形貌。結果表明:復合材料相對致密度隨制備溫度提高而增加,纖維局部偏聚現象也明顯減少,與此同時,界面反應物Al4C3相隨制備溫度提高而顯著增多,530℃到570℃復合材料室溫拉伸極限強度隨組織缺陷減少而增加,570℃到600℃復合材料室溫極限拉伸強度隨界面反應程度增大而顯著降低;高溫拉伸極限強度隨制備溫度提高而增加,適當提高界面反應程度有利于提高復合材料高溫力學性能,高溫拉伸中基體合金回復軟化和界面結合強度弱化促進了復合材料斷裂過程中的纖維拔出與界面滑移。"/>

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預熱溫度對三維五向Cf/Al復合材料微觀組織及室溫與高溫力學性能的影響
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南昌航空大學 輕合金加工科學與技術國防重點學科實驗室,南昌航空大學 輕合金加工科學與技術國防重點學科實驗室,南昌航空大學 輕合金加工科學與技術國防重點學科實驗室,南昌航空大學 輕合金加工科學與技術國防重點學科實驗室,中航工業(yè)北京航空材料研究院

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國家自然科學基金(51365043),凝固技術國家重點實驗室開放基金(SKLSP201228)和江西省自然科學基金(20151BAB206004)資助項目.


Effect of fabrication temperature on the microstructure and mechanical property of 3D fabric reinforced Cf/Al composites*
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Nanchang Hangkong University,Key discipline laboratory of light alloy processing science and technology,Nanchang Hangkong University,Key discipline laboratory of light alloy processing science and technology,Nanchang Hangkong University,Key discipline laboratory of light alloy processing science and technology,Nanchang Hangkong University,Key discipline laboratory of light alloy processing science and technology,AVIC,Beijing Institute of Aeronautical Materials

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    摘要:

    以石墨纖維三維五向織物為增強體,鋁合金ZL301為基體材料,采用真空輔助壓力浸滲法制備了三維五向增強Cf/Al復合材料,研究了不同溫度制備的復合材料微觀組織特征和界面反應程度,測試了復合材料在室溫和高溫下的拉伸力學性能并分析了其斷口形貌。結果表明:復合材料相對致密度隨制備溫度提高而增加,纖維局部偏聚現象也明顯減少,與此同時,界面反應物Al4C3相隨制備溫度提高而顯著增多,530℃到570℃復合材料室溫拉伸極限強度隨組織缺陷減少而增加,570℃到600℃復合材料室溫極限拉伸強度隨界面反應程度增大而顯著降低;高溫拉伸極限強度隨制備溫度提高而增加,適當提高界面反應程度有利于提高復合材料高溫力學性能,高溫拉伸中基體合金回復軟化和界面結合強度弱化促進了復合材料斷裂過程中的纖維拔出與界面滑移。

    Abstract:

    3D fabric reinforced Cf/Al composites were fabricated by the vacuum assisted pressure infiltration method. The microstructure and interfacial reaction of the composites prepared at different temperature levels was investigated. The uniaxial tensile property of the composites was tested at room temperature and elevated temperature and the corresponding tensile fracture surface was analyzed. The results indicated that the relative density increased and the fiber segregation in partial region decreased with fabrication temperature increasing. Meanwhile the content of Al4C3 compound at interface increased obviously. At room temperature, the ultimate tensile strength of the composites from 570℃ to 600℃ degenerated dramatically with interfacial reaction aggravated. When the composites were tested at elevated temperature, however, the ultimate tensile strength increased with fabrication temperature increasing. The improvement of interfacial strength is beneficial to the high temperature mechanical property. The matrix alloy softening and interface weakening due to elevated temperature can promote the fiber pull out and interface sliding during the fracture process.

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王振軍,朱世學,余歡,徐志鋒,陳新文.預熱溫度對三維五向Cf/Al復合材料微觀組織及室溫與高溫力學性能的影響[J].稀有金屬材料與工程,2018,47(3):982~989.[Wang Zhenjun, Zhu Shixue, Yu Huan, Xu Zhifeng, Chen Xinwen. Effect of fabrication temperature on the microstructure and mechanical property of 3D fabric reinforced Cf/Al composites*[J]. Rare Metal Materials and Engineering,2018,47(3):982~989.]
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  • 收稿日期:2016-01-14
  • 最后修改日期:2016-05-12
  • 錄用日期:2016-05-18
  • 在線發(fā)布日期: 2018-04-11
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