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球磨高氮不銹鋼粉末特性及注射喂料流變性能
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國家自然科學基金 (51004077);山東省優(yōu)秀中青年科學家獎勵基金 (BS2010CL046)


Characteristics of High Nitrogen Stainless Steel Powder by Milling and Rheological Properties of Its MIM Feedstock
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    摘要:

    采用高能球磨技術制備了高氮節(jié)鎳不銹鋼近球形復合粉末,與石蠟基多聚合物組元黏結劑混煉制成金屬注射成形喂料,研究了注射喂料的黏度、剪切速率以及溫度等對黏度的影響。結果表明:高能球磨能夠顯著改善高氮不銹鋼粉末的工藝特性,球磨60 h得到的粉末顆粒細小,球形度較好,振實密度高,適合用來制作高質量的金屬注射成形喂料。其中,粉末裝載量為58%的喂料應變敏感因子最小(n=0.45),粘流活化能最低(E=28.70 kJ/mol),綜合流變學因子最大(αSTV=2.96),表明該喂料具有最好的綜合流變性能,非常適宜進行后續(xù)注射成形工藝

    Abstract:

    Nearly spherical composite powders of high nitrogen nickel-saving stainless steel were synthesized by a high energy milling technique, and the MIM (metal injection molding) feedstock was prepared by mixing these metal powders with paraffin based multi-component binder. The rheological properties of MIM feedstock including feedstock viscosity and its sensitivity to the shear rate and the temperature were also investigated. The results show that the high energy milling can remarkably improve technological characteristics of the powders, and it is found that the powders milled for 60 h have fine particle size, good sphericity and high tap density, suitable for making high-quality MIM feedstock. The feedstock with powder loading of 58% presents the minimum shear rate sensitivity factor, the lowest viscous flow activation energy, and the largest general rheological index, which are n=0.45, E=28.70 kJ/mol and αSTV=2.96, respectively, exhibiting the best rheological properties and meeting process requirements for subsequent injection procedure very well

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崔大偉,曲選輝,魏文慶,劉炳強.球磨高氮不銹鋼粉末特性及注射喂料流變性能[J].稀有金屬材料與工程,2015,44(12):3173~3177.[Cui Dawei, Qu Xuanhui, Wei Wenqing, Liu Bingqiang. Characteristics of High Nitrogen Stainless Steel Powder by Milling and Rheological Properties of Its MIM Feedstock[J]. Rare Metal Materials and Engineering,2015,44(12):3173~3177.]
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  • 收稿日期:2014-12-07
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  • 在線發(fā)布日期: 2016-08-29
  • 出版日期: 2015-12-25