-1條件下,通過Gleeble熱力模擬試驗機對其進行了一系列恒溫壓縮實驗,結(jié)合組織觀察,研究了Y添加1.5wt%時對合金組織結(jié)構(gòu)、流變行為、本構(gòu)參數(shù)及高溫塑性變形行為的影響。研究顯示,Y細化了鑄態(tài)合金晶粒,三角晶界處共晶產(chǎn)物明顯增多、并演變?yōu)榍逦膲K狀、網(wǎng)狀結(jié)構(gòu);Y未對合金流變應力曲線的特征產(chǎn)生顯著影響,但引起流變應力水平、峰值應力普遍增大。根據(jù)雙曲正弦函數(shù),線性擬合確定了Y添加前后合金的本構(gòu)參數(shù),建立了定量描述流變應力同變形溫度和應變速率之間關(guān)系的本構(gòu)方程,其中Y使應力指數(shù)(n=5.778)、表觀變形激活能(Q=181.082)的平均值增幅超過14.2%和21.6%,表明Y導致合金塑性變形抗力增大。另外,高溫壓縮后的組織顯示,Y有利于促使合金發(fā)生動態(tài)再結(jié)晶,晶界處再結(jié)晶晶粒增多、晶粒尺寸更細小,表明含稀土Y第二相影響了晶界界面遷移。"/>

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稀土Y對鑄態(tài)ZK30鎂合金高溫塑性流變行為的影響
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內(nèi)蒙古工業(yè)大學,內(nèi)蒙古工業(yè)大學,內(nèi)蒙古工業(yè)大學;內(nèi)蒙古化工職業(yè)學院,內(nèi)蒙古工業(yè)大學,內(nèi)蒙古工業(yè)大學,內(nèi)蒙古工業(yè)大學

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TG146.4

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內(nèi)蒙古自治區(qū)自然科學基金資助(項目批準號:2013ZD10和2015MS0510)


Effects of Rare-earth Y Doping on the High-temperature Plastic FlowBehavior of As-cast ZK30 Magnesium Alloy
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Inner Mongolia University of Technology,Inner Mongolia University of Technology,Inner Mongolia University of Technology; Inner Mongolia Vocational College of Chemical Engineering,Inner Mongolia University of Technology,Inner Mongolia University of Technology,Inner Mongolia University of Technology

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    摘要:

    為了研究稀土釔(Y)對鑄態(tài)ZK30鎂合金高溫塑性變形行為的影響,在變形溫度為573~723 K、應變速率為0.001~1s-1條件下,通過Gleeble熱力模擬試驗機對其進行了一系列恒溫壓縮實驗,結(jié)合組織觀察,研究了Y添加1.5wt%時對合金組織結(jié)構(gòu)、流變行為、本構(gòu)參數(shù)及高溫塑性變形行為的影響。研究顯示,Y細化了鑄態(tài)合金晶粒,三角晶界處共晶產(chǎn)物明顯增多、并演變?yōu)榍逦膲K狀、網(wǎng)狀結(jié)構(gòu);Y未對合金流變應力曲線的特征產(chǎn)生顯著影響,但引起流變應力水平、峰值應力普遍增大。根據(jù)雙曲正弦函數(shù),線性擬合確定了Y添加前后合金的本構(gòu)參數(shù),建立了定量描述流變應力同變形溫度和應變速率之間關(guān)系的本構(gòu)方程,其中Y使應力指數(shù)(n=5.778)、表觀變形激活能(Q=181.082)的平均值增幅超過14.2%和21.6%,表明Y導致合金塑性變形抗力增大。另外,高溫壓縮后的組織顯示,Y有利于促使合金發(fā)生動態(tài)再結(jié)晶,晶界處再結(jié)晶晶粒增多、晶粒尺寸更細小,表明含稀土Y第二相影響了晶界界面遷移。

    Abstract:

    In order to improve the understanding of the effectSmechanism of rare earth yttrium (Y) element on the plastic deformation of as-cast ZK30 magnesium alloy, and to use it more effectively, carried out a series of isothermal compressive tests of specimens were performed in the deformation temperature range of 573~723 K, and the strain rate range of 0.001~1 s-1 on thermo-mechanical simulator. Combing with the microstructure observation, the effects of Y (1.5wt %) on the microstructure, flow behavior, constitutive parameters and high temperature plastic properties of the ZK30 magnesium alloy were investigated. According to the hyperbolic function, constitutive parameters of the alloy were obtained by linear fitting, a nonlinear flow model and its constitutive equation have been established and employed for studying the plastic deformation behavior and the relationship between temperature, strain rate and flow stress. The results showed that Y could refine the as-cast grain and increase the amount of eutectic intermetallic compound in grain boundaries. The Y doping could effectively enhance the flow stress level and peak stress, but the change trend of true stress-strain curves are less affected. The average activation energy (Q=181.082KJ.mol-1) and stressSexponent (n=5.778) for the plastic deformation have been determinded, enlarged by 14.2% and 21.6%, respectively. The resultsSshow that theSplastic deformationSresistanceSof theSalloySis enhanced. Combined with metallurgy microstructure of these samples after deformation, Y could refine the grain and increase the amount of the dynamic recrystallization in triangle boundaries. The results showed that Y was facilitatingSdynamicSrecrystallization occur, and it was influencing theSmechanism of interface migration.

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陳寶東,郭 鋒,溫 靜,馬 文,蔡會生,劉亮.稀土Y對鑄態(tài)ZK30鎂合金高溫塑性流變行為的影響[J].稀有金屬材料與工程,2017,46(12):3811~3817.[Chen Baodong, Guo Feng, Wen Jing, Ma Wen, Cai Huisheng, Liu Liang. Effects of Rare-earth Y Doping on the High-temperature Plastic FlowBehavior of As-cast ZK30 Magnesium Alloy[J]. Rare Metal Materials and Engineering,2017,46(12):3811~3817.]
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  • 收稿日期:2015-10-26
  • 最后修改日期:2016-01-03
  • 錄用日期:2016-01-14
  • 在線發(fā)布日期: 2018-01-04
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