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循環(huán)載荷下表面強(qiáng)化工業(yè)純鋯殘余應(yīng)力釋放研究
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國家自然科學(xué)基金青年基金(51104114);國家自然科學(xué)基金(51274160);碑林區(qū)科技局科技計(jì)劃項(xiàng)目; 陜西省教育廳科技項(xiàng)目 (13JS061)


Residual Stress Relaxation of Surface Strengthened Commercial Pure Zirconium under Cycle Load
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    摘要:

    對(duì)工業(yè)純鋯進(jìn)行表面機(jī)械研磨處理(SMAT),實(shí)現(xiàn)其表面納米化,并引入殘余壓應(yīng)力場。采用偏光顯微鏡(PM)、透射電子顯微鏡(TEM)對(duì)SMAT處理試樣顯微組織進(jìn)行表征,利用X射線應(yīng)力儀測試不同循環(huán)加載周次下距試樣表面不同深度處宏觀殘余應(yīng)力。研究不同循環(huán)加載周次下距表層不同深度處X射線衍射峰半高寬的變化特征,并采用Voigt函數(shù)擬合X射線衍射峰,得到微觀應(yīng)變和位錯(cuò)密度的分布特征。結(jié)果表明:循環(huán)加載初期殘余應(yīng)力釋放率最大,約為25%,隨著循環(huán)加載周次增加殘余應(yīng)力釋放率趨于穩(wěn)定;不同循環(huán)加載周次下,隨距表層深度增加,X射線衍射峰半高寬、微觀應(yīng)變和位錯(cuò)密度逐漸降低后趨于穩(wěn)定;隨著位錯(cuò)密度降低,殘余壓應(yīng)力逐漸增加,位錯(cuò)密度值穩(wěn)定于約2×1010 cm-2時(shí)所對(duì)應(yīng)的深度,和最大殘余壓應(yīng)力對(duì)應(yīng)的深度基本一致。循環(huán)載荷下殘余應(yīng)力釋放是通過微觀塑性變形過程中位錯(cuò)運(yùn)動(dòng)來實(shí)現(xiàn)

    Abstract:

    The commercial pure zirconium samples were processed by surface mechanical attrition treatment (SMAT) to realize the surface nanocrystallization, and the compressive residual stress was induced at the same time. The microstructure was studied by PM and TEM after SMAT. The macroscopic residual stress at different depths from surface was evaluated by XRD after different cycles. The distribution characteristics of FWHM were investigated. Fitting the peaks from XRD by Voigt function, microstrain and dislocation density at different depths from top surface after different cycles were obtained. The results indicate that the biggest relaxation rate (about 25%) is found at initial stage, and the more cycles, the less residual stress relaxation. Under different cycles, with the increase of the depth from the top surface, the FWHM decreases rapidly, and then reaches to a steady state. The distribution characteristics of the microstrain and dislocation density at different depths from surface are similar to FWHM after different cycles. Along with the decrease of dislocation density, the residual stress increases gradually. The depth where the dislocation density value is about 2×1010 cm-2 is similar to that of the maximum compressive residual stress. The residual stress relaxation is achieved by the accumulation of plastic deformation in the process of dislocation motion under cyclic loading

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張聰惠,宋 薇,朱姍姍,王耀勉,王 洋.循環(huán)載荷下表面強(qiáng)化工業(yè)純鋯殘余應(yīng)力釋放研究[J].稀有金屬材料與工程,2015,44(10):2513~2518.[Zhang Conghui, Song Wei, Zhu Shanshan, Wang Yaomian, Wang Yang. Residual Stress Relaxation of Surface Strengthened Commercial Pure Zirconium under Cycle Load[J]. Rare Metal Materials and Engineering,2015,44(10):2513~2518.]
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  • 收稿日期:2014-10-22
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  • 在線發(fā)布日期: 2016-07-13
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