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生長速率對鎂合金微弧氧化膜結(jié)構(gòu)及耐蝕性的影響
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蘭州理工大學(xué),蘭州理工大學(xué),蘭州理工大學(xué),蘭州理工大學(xué),蘭州理工大學(xué),蘭州理工大學(xué)

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TG174

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材料腐蝕與防護四川省重點實驗室開放基金(2012CL08)


Effect of Growth Rate on Microstructure and Corrosion Resistance of Micro-arc Oxidation Coatings on Magnesium Alloy
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Lanzhou University of Technology,,,,,

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    摘要:

    硅酸鹽電解液體系中對AZ91D鎂合金進行微弧氧化處理,膜層厚度相同但生長速率不同是本研究的實驗設(shè)計特色。通過調(diào)節(jié)電源電壓,使得膜層的生長速率分別為1μm/min、5μm/min、15μm/min和25μm/min,從而制備出生長速率不同但厚度相同的微弧氧化膜層,對膜層的微觀結(jié)構(gòu)及耐蝕性進行定性及定量研究,從實驗室研究及實際應(yīng)用角度對不同生長速率的各膜層進行綜合對比分析。結(jié)果表明,生長速率對膜層的表面孔隙率、微孔的尺寸及數(shù)量,膜層的質(zhì)量及質(zhì)量厚度比,以及膜層耐蝕性均有較大的影響,但對膜層中的成分及元素分布基本無影響;在工業(yè)應(yīng)用中,膜層生長速率的選擇,應(yīng)將膜層的生產(chǎn)效率和膜層性能統(tǒng)籌考量,本研究中生長速率為15μm/min的膜層顯示出這樣的優(yōu)勢。

    Abstract:

    AZ91D magnesium alloys were processed by micro-arc oxidation (MAO) in silicate-containing electrolyte. The key factor of this research is a unique experimental design to fabricate coatings with same thickness but by different power voltages which represents different growth rate. The fact, that the coatings with same thickness corresponding to different coating growth rate of 1μm/min, 5μm/min, 15μm/min and 25μm/min respectively, makes the comparison and analysis-targeted microstructure and corrosion resistance of the coatings academic and practical. The coating growth rate demonstrates considerable influence on surface porosity, size and amount of micro-pores, mass and mass to thickness ratio, and anti-corrosion property of the coatings based on both qualitative and quantitative analysis, but it is not the case for the composition and element distribution of the coatings. An industrial application-oriented selection of appropriate coating growth rate, which demands for both productive efficiency and good performance, has to be considered together with anti-corrosion property of the coatings. The case of the coating fabricated with the growth rate of 15μm/min supports this point strongly.

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董海榮,馬穎,王晟,趙曉鑫,郭惠霞,郝遠.生長速率對鎂合金微弧氧化膜結(jié)構(gòu)及耐蝕性的影響[J].稀有金屬材料與工程,2017,46(9):2399~2404.[Dong Hairong, Ma Ying, Wang Sheng, Zhao Xiaoxin, Guo Huixia, Hao Yuan. Effect of Growth Rate on Microstructure and Corrosion Resistance of Micro-arc Oxidation Coatings on Magnesium Alloy[J]. Rare Metal Materials and Engineering,2017,46(9):2399~2404.]
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  • 收稿日期:2015-09-18
  • 最后修改日期:2015-12-11
  • 錄用日期:2015-12-11
  • 在線發(fā)布日期: 2017-11-29
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