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電鑄鎳工藝參數(shù)對(duì)鑄鎳層組織和性能的影響
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航空科學(xué)基金(2012ZE51058)


Effect of Technology Parameters on Microstructure and Properties of Electroforming Nickel Layer
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    摘要:

    利用凈化的氨基磺酸鹽溶液體系,分別采用金相顯微鏡、陰極彎曲法和拉伸試驗(yàn)的方法研究了陰極電流密度、溶液溫度和pH值等工藝參數(shù)對(duì)電鑄鎳層的組織形貌、內(nèi)應(yīng)力和力學(xué)性能(抗拉強(qiáng)度、延伸率)的影響。結(jié)果表明:電鑄鎳的工藝參數(shù)影響鑄鎳層的組織結(jié)構(gòu),進(jìn)而影響到鑄鎳層的性能;鑄鎳層的晶粒隨陰極電流密度的降低和溶液溫度的升高而細(xì)化,同時(shí)當(dāng)溶液pH值為4.0時(shí),也可以獲得較細(xì)的晶粒;隨著晶粒的細(xì)化,鑄鎳層的內(nèi)應(yīng)力降低,抗拉強(qiáng)度升高而延伸率降低;通過(guò)優(yōu)化工藝參數(shù),獲得了抗拉強(qiáng)度為673 MPa、延伸率為23.2%和內(nèi)應(yīng)力為48 MPa的綜合性能優(yōu)異的鑄鎳層。

    Abstract:

    Electroforming nickel was prepared from a purified sulfamate system. The effects of cathode-current density, temperature and pH of the solution on the microstructure, internal stress and mechanical properties (tensile strength and elongation) of electroforming nickel layer were investigated by metallographic microscope, cathode bending method and tensile test. The results show that the properties of electroforming nickel layer are influenced by microstructure, while the microstructure is influenced by electroforming parameters; the grain size of electroforming nickel decreases with the decrease of cathode-current density or the increase of temperature; when the pH is 4.0, the grain diminishes too; with the decrease of the grain size, the tensile strength of electroforming nickel layer increases while internal stress and elongation decrease. By optimizing technology parameters, the electroforming nickel layer with excellent properties are prepared, including the tensile strength of 673 MPa, elongation of 23.2% and internal stress of 48 MPa.

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錢建剛,李海婷,李彭瑞.電鑄鎳工藝參數(shù)對(duì)鑄鎳層組織和性能的影響[J].稀有金屬材料與工程,2015,44(7):1758~1762.[Qian Jiangang, Li Haiting, Li Pengrui. Effect of Technology Parameters on Microstructure and Properties of Electroforming Nickel Layer[J]. Rare Metal Materials and Engineering,2015,44(7):1758~1762.]
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  • 收稿日期:2014-07-20
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  • 在線發(fā)布日期: 2016-01-04
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