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定向凝固含Y鎂合金的枝晶形態(tài)及微觀組織研究
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江西省鎂合金工程研究中心,江西省鎂合金工程研究中心,江西省鎂合金工程研究中心,江西省鎂合金工程研究中心

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國(guó)家自然科學(xué)基金資助(項(xiàng)目號(hào)51464002),江西省科技落地計(jì)劃項(xiàng)目(項(xiàng)目號(hào)KJLD13078)


Dendrite morphology and microstructure in directionalloy solidified Mg alloy with rare earth element Y
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Jiangxi Engineering Research Center for Magnesium Alloys,,,

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    摘要:

    采用液態(tài)金屬冷卻高溫度梯度定向凝固爐制備了含稀土元素Y的鎂合金,研究了定向凝固鎂合金的枝晶形態(tài)及微觀組織特征。結(jié)果表明,鎂合金的一次枝晶沿著熱流方向生長(zhǎng),且一次枝晶周圍含有六個(gè)二次枝晶呈花瓣形狀。通過掃描電鏡及能譜分析發(fā)現(xiàn),凝固組織中除了a(Mg)固溶體及枝晶間的?(Mg17Al12)相組成外,還存在稀土相。稀土相呈粗大的桿狀和細(xì)小的粒狀形態(tài),主要由Y、Mg、Al和Mn元素組成,其中稀土Y的質(zhì)量分?jǐn)?shù)占22%左右。

    Abstract:

    Directionally solidified Manesium alloys AZ91 with element Y were produced by using the liquid metal cooling Bridgman furnance. The dendrite morphology and microstructure of AZ91 were investigated in present paper. The results indicated that the primary dendrites of AZ91 grow along the direction of heat flow. The are six secondary dendrites which around the primary dendrite likes petal shape can be observed in cross section. The microstructure of AZ91 alloy is mainly composed of a matrix of primary a(Mg) solid solution and eutectic b(Mg17Al12) phase, and some Y-rich phase can be found with Y additions by using SEM and EDS. The RE-rich phases present coarse rod-like shape or tiny graininess. The Y, Mg, Al and Mn elements are found in RE-rich phase, and the mass fraction of rare earth element Y is about 22%.

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楊初斌,羅寧,張小聯(lián),韓寶軍.定向凝固含Y鎂合金的枝晶形態(tài)及微觀組織研究[J].稀有金屬材料與工程,2017,46(10):3028~3032.[Yang Chubin, Luo Ning, Zhang Xiaolian, Han Baojun. Dendrite morphology and microstructure in directionalloy solidified Mg alloy with rare earth element Y[J]. Rare Metal Materials and Engineering,2017,46(10):3028~3032.]
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  • 收稿日期:2015-06-11
  • 最后修改日期:2015-08-10
  • 錄用日期:2015-09-07
  • 在線發(fā)布日期: 2017-12-01
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