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時效預處理態(tài)Al-Zn-Mg-Cu合金熱變形及其后熱處理過程中晶粒組織的演變
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國家自然科學基金項目 (51175361);山西省科技攻關項目 (20110321013-02);太原市科技明星項目 (120247-1)


Grain Evolution during Hot Deformation and Subsequent Heat Treatments Processes of As-aging Pre-treated Al-Zn-Mg-Cu Alloy
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    摘要:

    以435 ℃/2 h+200 ℃/12 h固溶時效預處理的新型Al-Zn-Mg-Cu高強鋁合金為研究對象,在溫度350~400 ℃,應變速率0.01~1 s-1和變形量60%~80%條件下進行熱壓縮變形,再經(jīng)350 ℃/0.5 h+470 ℃/2 h退火和固溶處理。采用光學(OM)、電子顯微鏡(EBSD、TEM)組織觀察和測試方法,研究了時效預處理析出相粒子對熱壓縮變形及隨后退火和固溶處理過程中晶粒組織的演變機理和規(guī)律。結(jié)果表明:(1)在400 ℃、0.05 s-1、60%條件下,lnZ值為24.33,發(fā)生了連續(xù)動態(tài)再結(jié)晶,獲得了細小均勻的再結(jié)晶晶粒組織;經(jīng)退火和固溶處理后,晶粒趨于等軸狀,尺寸稍有增加,最終獲得細小均勻的晶粒組織。(2)在380 ℃、0.1 s-1、60%條件下,lnZ值增加到25左右,晶粒沿變形方向拉長,晶界斷續(xù)分布著細小的再結(jié)晶晶粒;經(jīng)退火和固溶處理后,晶粒長大不明顯,在變形拉長的晶粒內(nèi)部均勻分布著尺寸較小的回復亞晶粒。(3)當應變速率較快或變形溫度較低,lnZ值增加到約26,且變形量較大時,動態(tài)再結(jié)晶不明顯,晶粒沿變形方向劇烈拉長;經(jīng)退火和固溶處理處理后,晶粒長大明顯,最終獲得粗大的晶粒組織

    Abstract:

    A new Al-Zn-Mg-Cu high strength aluminum alloy after solution and aging pre-treatments of 435 oC/2 h+200 oC/12 h was taken as the object and hot compressions at temperatures in the range of 350~400 oC, strain rates in the range of 0.01 to 1 s-1 and height reduction up to 60%~80% were carried out followed by subsequent annealing and solution treatments of 350 oC/0.5 h+470 oC/2 h. The influences of precipitated particles on grain evolution mechanisms and regulations during hot deformation and subsequent annealing and solution treatments were investigated by optical microscope (OM) and electronic microscope (EBSD, TEM). The conclusions can be drawn as following. (i) Continuous dynamic recrystallization occurs under deformation conditions of 400 ℃, 0.05 s-1, 60%, the value of lnZ is 24.33, and refined and uniform recrystallized grains appear. After subsequent annealing and solution treatments, recrystallized grains become more equiaxed and uniform, and the size of grains increases slightly. As a result, the refined, equiaxed and uniformly-distributed grain structure occurs. (ii) When hot compression is carried out under conditions of 380 oC, 0.1 s-1, 60%, the value of lnZ increases to 25 or so, grains are elongated along the deformation direction with some refined recrystallized grains at the grain-boundaries. After subsequent annealing and solution treatments, grain growth is not too much, and refined and recovered well sub-grains come forth evenly in the elongated grains. As a result, the elongated grain structure with refined and uniform sub-grains emerges. (iii) At other conditions of increased strain rates or decreased temperatures, the value of lnZ increases to about 26, and deformation increases to large values, dynamic recrystallization can not be observed obviously and the prior grains are elongated severely. After subsequent annealing and solution treatments, the grains grow rapidly. As a result, the coarse grain structure appears

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趙曉東,韓連華,陳慧琴,路瑞龍,劉建生.時效預處理態(tài)Al-Zn-Mg-Cu合金熱變形及其后熱處理過程中晶粒組織的演變[J].稀有金屬材料與工程,2015,44(4):982~988.[Zhao Xiaodong, Han Lianhua, Chen Huiqin, Lu Ruilong, Liu Jiansheng. Grain Evolution during Hot Deformation and Subsequent Heat Treatments Processes of As-aging Pre-treated Al-Zn-Mg-Cu Alloy[J]. Rare Metal Materials and Engineering,2015,44(4):982~988.]
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  • 收稿日期:2014-04-17
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  • 在線發(fā)布日期: 2015-06-08
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