-1~10s-1的變形條件下,研究了大規(guī)格鑄錠晶粒尺寸的不均勻性對新型高強Al-7.68Zn-2.12Mg-1.98Cu-0.12Zr合金熱變形行為的影響。掃描電鏡(SEM)觀察表明,大鑄錠表層的晶粒尺寸比心層細小。熱變形過程中,細晶組織(鑄錠表層)的流變應力在高溫和低應變速率條件下低于粗晶組織(鑄錠心層。計算得到表層和心層組織的熱變形激活能分別為140kJ/mol和125.4kJ/mol?;谖诲e密度理論,利用一種兩階段型本構方程分別預測了粗晶和細晶組織的流變應力, 并建立了不同晶粒度組織的動態(tài)再結晶軟化方程。電子背散射衍射(EBSD)觀察表明,合金在300 ℃~400℃條件下發(fā)生動態(tài)回復,在450℃和低應變速率速(≤0.1s-1)條件下出現(xiàn)動態(tài)再結晶(DRX)現(xiàn)象,動態(tài)再結晶晶粒在原始大角度晶界上形核。由于表層(細晶)組織的晶界密度高,因此其動態(tài)再結晶程度高于心層(粗晶)組織。"/>

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晶粒尺寸對新型高強鋁合金熱變形行為的影響
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江蘇科技大學 材料科學與工程學院,中南大學,中南大學,蘇州有色金屬研究院有限公司

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TG146.2

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國家重點基礎研究發(fā)展計劃(項目號2012CB619500);江蘇高校優(yōu)勢學科建設工程資助項目


The Effect of Grain Size on Hot Deformation Behavior of a New High Strength Aluminum Alloy
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Jiangsu University of Science and Technology,,Central South University,Suzhou Nonferrous Metals Research Institute

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    摘要:

    利用Gleeble-3500試驗機,在300℃~450℃和0.1s-1~10s-1的變形條件下,研究了大規(guī)格鑄錠晶粒尺寸的不均勻性對新型高強Al-7.68Zn-2.12Mg-1.98Cu-0.12Zr合金熱變形行為的影響。掃描電鏡(SEM)觀察表明,大鑄錠表層的晶粒尺寸比心層細小。熱變形過程中,細晶組織(鑄錠表層)的流變應力在高溫和低應變速率條件下低于粗晶組織(鑄錠心層。計算得到表層和心層組織的熱變形激活能分別為140kJ/mol和125.4kJ/mol?;谖诲e密度理論,利用一種兩階段型本構方程分別預測了粗晶和細晶組織的流變應力, 并建立了不同晶粒度組織的動態(tài)再結晶軟化方程。電子背散射衍射(EBSD)觀察表明,合金在300 ℃~400℃條件下發(fā)生動態(tài)回復,在450℃和低應變速率速(≤0.1s-1)條件下出現(xiàn)動態(tài)再結晶(DRX)現(xiàn)象,動態(tài)再結晶晶粒在原始大角度晶界上形核。由于表層(細晶)組織的晶界密度高,因此其動態(tài)再結晶程度高于心層(粗晶)組織。

    Abstract:

    The effects of grain size inhomogeniety in large size ingot on hot deformation behaviors of a new high strength Al-7.68Zn-2.12Mg-1.98Cu-0.12Zr alloy were investigated using Gleeble-3500 test machine at 300–450℃ with strain rates from 0.1 to 10 s-1.SEM observation showed that the grain size in surface layer of ingot was finer than that in central layer. During hot deformation, the low stress of the sample with fine grain(surface layer) was lower than that of the sample with coarse grain(central layer)at high temperature and low strain rate conditions. The hot deformation activation energies(Q) of 140kJ/mol and 125.4kJ/mol were obtained for fine grain microstructure and coarse grain microstructure respectively. Thelow stresses were predicted by a two-stage type constitutive model based on the dislocation density theory, and the dynamic recrystallization soften equations were established for the microstructures of fine grain and coarse grain. Electron Back-Scattered Diffraction(EBSD) observations revealed that the alloy exhibited dynamic recovery at temperatures ranging from 300 to 400℃ and dynamic recrystallization(DRX) at 450℃ with low strain rate(≤0.1s-1).The DRX grains nucleated at the original grainSboundaries. It was found that the DRX fracture was higher in finer grain (surface layer)microstructure resulting from the higher grain boundary density.

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馮 迪,張新明,劉勝膽,韓念梅.晶粒尺寸對新型高強鋁合金熱變形行為的影響[J].稀有金屬材料與工程,2016,45(8):2104~2110.[Feng Di, Zhang Xinming, Liu Shengdan, Han Nianmei. The Effect of Grain Size on Hot Deformation Behavior of a New High Strength Aluminum Alloy[J]. Rare Metal Materials and Engineering,2016,45(8):2104~2110.]
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  • 收稿日期:2015-03-30
  • 最后修改日期:2015-06-04
  • 錄用日期:2015-08-11
  • 在線發(fā)布日期: 2016-10-09
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