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納米Cr2O3微粒對(duì)2024-T4微弧氧化膜結(jié)構(gòu)及耐磨性能的影響
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哈爾濱工業(yè)大學(xué),哈爾濱工業(yè)大學(xué)

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Effect of Nano Cr2O3 Particles on Microstructure and Wear Resistanceof Micro-arc Oxidation Coatings on 2024-T4 Aluminum Alloy
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    摘要:

    摘 要: 在含有不同濃度納米Cr2O3微粒的硅酸鹽體系電解液中對(duì)2024-T4鋁合金進(jìn)行微弧氧化處理,使用SEM觀察陶瓷膜的表面形貌和截面形貌,使用EDS能譜儀分析膜層中各主要成分沿截面方向的分布,使用XRD分析陶瓷膜的相結(jié)構(gòu),使用納米壓痕硬度計(jì)測(cè)量陶瓷膜的硬度,使用粗糙度儀測(cè)量陶瓷膜的表面粗糙度,使用摩擦磨損試驗(yàn)機(jī)測(cè)量陶瓷膜的摩擦系數(shù),使用激光共聚焦顯微鏡測(cè)量磨痕體積,評(píng)估磨損率,使用SEM觀察磨痕形貌,結(jié)果表明:在電解液中加入納米Cr2O3微粒后,制備的陶瓷膜中出現(xiàn)了Cr2O3相,電解液中納米Cr2O3微粒濃度達(dá)到2.4g/L時(shí),陶瓷膜的硬度最高,摩擦系數(shù)最小,磨損率最低,耐磨性最好。

    Abstract:

    Abstract: 2024-T4 aluminum alloy was treated by micro-arc oxidation in the silicate system electrolyte with different concentrations of nano Cr2O3 microparticles. The surface morphology and the cross-section morphology of ceramic coatings were observed by SEM. The distribution of main component of ceramic coatings along the cross-section was analyzed by EDS, and the phase structure of ceramic coatings was analyzed by XRD. The hardness of ceramic coatings was measured by nano indentation hardness tester. The surface roughness of ceramic coatings was measured by roughness meter. The friction coefficient of ceramic coatings was measured by Friction and wear tester. The wear volume of ceramic coatings were measured by laser confocal microscope and the wear rate was evaluated. The morphology of wear tracks was observed by SEM. The results show that the composition of Cr2O3 was discovered in the ceramic coatings after nano Cr2O3 microparticles were added to the electrolyte. The hardness of ceramic coatings is the highest, the friction coefficient of ceramic coatings is the minimum, the wear rate is the lowest, and the wear resistance of ceramic coatings is the best under the condition of concentration of nano Cr2O3 microparticles being 2.4 g/L in the electrolyte.

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李振偉,狄士春.納米Cr2O3微粒對(duì)2024-T4微弧氧化膜結(jié)構(gòu)及耐磨性能的影響[J].稀有金屬材料與工程,2017,46(7):2022~2027.[lizhenwei, dishichun. Effect of Nano Cr2O3 Particles on Microstructure and Wear Resistanceof Micro-arc Oxidation Coatings on 2024-T4 Aluminum Alloy[J]. Rare Metal Materials and Engineering,2017,46(7):2022~2027.]
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  • 收稿日期:2015-03-18
  • 最后修改日期:2015-09-29
  • 錄用日期:2015-10-13
  • 在線發(fā)布日期: 2017-11-14
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