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熱處理對擠壓鑄造n-SiCp/AZ91D鎂基復(fù)合材料組織和力學(xué)性能的影響
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清華大學(xué)自主科研計(jì)劃(20111080980);國家高技術(shù)研究發(fā)展計(jì)劃(“863”計(jì)劃)項(xiàng)目(2013AA031201)


Effect of Heat Treatment on Microstructure and Mechanical Properties
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    摘要:

    采用金相、X射線衍射、掃描電鏡(SEM)、拉伸試驗(yàn)等方法分析和測試了擠壓鑄造納米SiC顆粒增強(qiáng)AZ91D鎂基復(fù)合材料在鑄態(tài)(F)、固溶態(tài)(T4)和人工時(shí)效態(tài)(T6)下的組織和力學(xué)性能。結(jié)果表明,固溶處理可使n-SiCp/AZ91D鑄態(tài)組織中的β-Mg17Al12共晶相溶入到基體中,形成單一的過飽和α-Mg固溶體,合金抗拉強(qiáng)度和伸長率均有大幅提高,分別達(dá)到265 MPa 和13.7%;經(jīng)時(shí)效處理后,復(fù)合材料的抗拉強(qiáng)度和屈服強(qiáng)度進(jìn)一步提高,分別為275,145 MPa;SEM結(jié)果顯示,β-Mg17Al12相主要以連續(xù)析出/非連續(xù)析出方式分別在晶內(nèi)及晶界上析出,特別是納米SiC顆粒分布對二次析出相β-Mg17Al12的形貌、尺寸、分布有一定的影響,使二次析出相變得細(xì)小和彌散分布,從而充分發(fā)揮了二次析出相的沉淀強(qiáng)化作用;最后對n-SiCp/AZ91D復(fù)合材料不同熱處理?xiàng)l件下的斷口形貌進(jìn)行了SEM觀察,并且對其斷裂方式進(jìn)行了分析和討論

    Abstract:

    Magnesium matrix composite reinforced with SiC nanoparticles (n-SiCp/AZ91D) was fabricated by squeeze casting. The microstructure and mechanical properties of the nanocomposite at as-cast state (F), solid solution state (T4) and artificial aging state (T6) were investigated by optical microscopy, X-ray diffraction, scanning electronic microscopy (SEM) and tensile tests. The results show that the solid solution treatment can dissolve the β-Mg17Al12 eutectic phase in the matrix of n-SiCp/AZ91D composites to produce single supersaturated solid solution α-Mg phase and the ultimate tensile strength and elongation are significantly improved which can be up to 265 MPa and 13.7%, respectively. After aging treatment, the ultimate tensile strength and yield strength of the nanocomposite are further improved, which is 275 MPa and 145 MPa, respectively. SEM results show that the β-Mg17Al12 phase is mainly precipitated in grain and at grain boundary as continuous or non continuous forms. In particular SiC nanoparticles have an important effect on the morphology, size and distribution of the β-Mg17Al12 precipitation phase and they result in the fine and uniformly dispersed secondary precipitate phase to be formed, which gives full play to the secondary precipitation strengthening effect. Finally, the fracture morphology of n-SiCp/AZ91D composites at different heat treatment conditions were observed by SEM and the fracture behavior were analyzed and discussed

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張從陽,馮榮宇,李文珍.熱處理對擠壓鑄造n-SiCp/AZ91D鎂基復(fù)合材料組織和力學(xué)性能的影響[J].稀有金屬材料與工程,2015,44(2):463~468.[Zhang Congyang, Feng Rongyu, Li Wenzhen. Effect of Heat Treatment on Microstructure and Mechanical Properties[J]. Rare Metal Materials and Engineering,2015,44(2):463~468.]
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  • 收稿日期:2014-01-15
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  • 在線發(fā)布日期: 2015-05-29
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