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B4C/6061Al中子吸收材料FSW接頭的納米壓痕和拉伸性能研究
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太原理工大學(xué),太原理工大學(xué)

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中圖分類(lèi)號(hào):

TG77

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山西省科技攻關(guān)項(xiàng)目,太原理工大學(xué)研究生科技創(chuàng)新項(xiàng)目


Nanoindentation and tensile properties of B4C/6061Al neutron absorbers
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Taiyuan University of Technology,Taiyuan University of Technology

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    摘要:

    高B4C含量的Al基復(fù)合材料由于其優(yōu)良的中子吸收性能被應(yīng)用于核電乏燃料池的貯存格架,采用傳統(tǒng)熔化焊方法由于凝固引起的結(jié)構(gòu)變化和產(chǎn)生化學(xué)反應(yīng)顯著降低了焊接接頭的性能。本文采用粉末冶金的方法制備了30vol.?C/6061Al中子吸收材料板材。通過(guò)攪拌摩擦焊(FSW)的方法對(duì)4 mm厚30vol.% B4C/6061Al中子吸收材料板材進(jìn)行對(duì)接焊接,獲得了表面成形良好的焊縫。采用納米壓痕法對(duì)FSW焊接接頭的焊核(WZ)、熱力影響區(qū)(TMAZ)、熱影響區(qū)(HAZ)和母材(BM)四個(gè)區(qū)域中的微區(qū)力學(xué)性能進(jìn)行研究,對(duì)焊接接頭的拉伸性能進(jìn)行了測(cè)試。運(yùn)用掃描電鏡對(duì)壓痕的微觀形貌和拉伸斷口進(jìn)行了表征。結(jié)果表明:在同一區(qū)域中,隨著距顆粒/基體界面距離d(d<11 μm)的增加,微區(qū)的硬度和彈性模量總體呈現(xiàn)減小的趨勢(shì)。在微區(qū)均值化后,不同區(qū)域的硬度和彈性模量由高到低為WZ、TMAZ、BM和HAZ,壓入功恢復(fù)率在WZ、TMAZ、HAZ和BM依次為28.10%、25.14%、31.76%和29.30%。在焊接接頭不同區(qū)域出現(xiàn)性能差別的原因是由于在FSW過(guò)程中不同區(qū)域的塑性變形程度和熱循環(huán)作用不同導(dǎo)致的,F(xiàn)SW接頭強(qiáng)度可達(dá)母材的85.7%,斷裂部位在HAZ區(qū)。

    Abstract:

    Aluminum with a high B4C content are valuable as a neutron absorber for spent nuclear fule pool storage rack,welding of B4C/6061Al using conventional fusion methods degrades the joint properties due to solidification induced structure and chemical reactions. B4C/6061Al neutron absorbers were fabricated by powder metallurgy with the B4C volume fractions of 0 ~ 30%. Plates of 4 mm thickness and 30% B4C/6061Al neutron absorbers was prepared and successfully butt joined using friction stir welding (FSW). The weld displays the smooth appearance. The micro-mechanical properties in welded joints of FSW weld nugget (WZ), Thermo-mechanically affected zone (TMAZ), heat affected zone (HAZ) and base metal (BM) were investigated by nanoindentation method, and the tensile tests were carried out.Furthermore,the microstructure of indentation and fracture surface were characterized by scanning electron microscope. The results showed that in the same region, with the distance(d<11 μm) of the interface between particle and matrix increased, the micro-area of hardness and elastic modulus decreased overall. After the micro-area equalization, different regions of hardness and elastic modulus from high to low were WZ, TMAZ, BM and HAZ. The pressure into the power recovery rate in WZ, TMAZ, HAZ and BM were 28.10%, 25.14%, 31.76% and 29.30%. The performance difference in the welding joint of different areas was caused by the different degree of plastic deformation and the thermal cycle in different area. A joint efficiency of 85.7% was realized under the experimental conditions, and the welded joint failed at HAZ.

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陳洪勝,王文先. B4C/6061Al中子吸收材料FSW接頭的納米壓痕和拉伸性能研究[J].稀有金屬材料與工程,2017,46(2):392~398.[chenhongsheng, wangwenxian. Nanoindentation and tensile properties of B4C/6061Al neutron absorbers[J]. Rare Metal Materials and Engineering,2017,46(2):392~398.]
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  • 收稿日期:2014-10-27
  • 最后修改日期:2015-05-04
  • 錄用日期:2015-06-11
  • 在線發(fā)布日期: 2017-04-10
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