最新色国产精品精品视频,中文字幕日韩一区二区不卡,亚洲有码转帖,夜夜躁日日躁狠狠久久av,中国凸偷窥xxxx自由视频

+高級檢索
機(jī)械固相化學(xué)反應(yīng)制備納米β-Co粉及其反應(yīng)熱力學(xué)研究
DOI:
作者:
作者單位:

作者簡介:

通訊作者:

中圖分類號:

基金項目:

重慶市教委科學(xué)技術(shù)研究項目 (KJ121217,KJ121203)


State Key Laboratory for Powder Metallurgy, Central South University, Changsha 410083, China
Author:
Affiliation:

Fund Project:

  • 摘要
  • |
  • 圖/表
  • |
  • 訪問統(tǒng)計
  • |
  • 參考文獻(xiàn)
  • |
  • 相似文獻(xiàn)
  • |
  • 引證文獻(xiàn)
  • |
  • 資源附件
  • |
  • 文章評論
    摘要:

    以H2C2O4·2H2O及Co(NO3)2·6H2O為原料,在高速球磨中進(jìn)行固相化學(xué)反應(yīng),經(jīng)洗滌并噴霧干燥獲得分布均勻的球形納米晶前驅(qū)物,再經(jīng)高溫分解,制備出目標(biāo)物。對分解產(chǎn)物進(jìn)行了XRD/SEM分析。結(jié)果表明,產(chǎn)物形貌為球形、平均粒徑在100 nm左右的納米粉體,其晶型為面心立方結(jié)構(gòu)β-Co,同時對制備反應(yīng)進(jìn)行了熱力學(xué)的研究

    Abstract:

    Pure nano-crystalline Co powders of nearly spherical shape have been produced using a high-energy ball mill. This method has used the mechanical force to crush solid reactant, which increased the BET specific surface area and reaction speed of reactant, and accelerated the nucleation rate. The method includes three steps. Firstly, a precursor of CoC2O4 was prepared by the mechano-chemical solid state reaction with H2C2O4·2H2O and Co(NO3)2·6H2O at ambient temperature. Secondly, the precursor CoH2C2O4 powders were dispersed by spray-drying to get the spherical precursor. Finally, Co powders were obtained by decomposition of the precursor CoH2C2O4 for about 3~3.5 h at 450~500 oC. The powders were characterized by X-ray diffractometer and scanning electron microscopy. The results show that spherical, cubic structure, 100 nm β-Co powders were synthesized

    參考文獻(xiàn)
    相似文獻(xiàn)
    引證文獻(xiàn)
引用本文

鄧 瑩,熊 翔,張艷華,涂銘旌,李 婧.機(jī)械固相化學(xué)反應(yīng)制備納米β-Co粉及其反應(yīng)熱力學(xué)研究[J].稀有金屬材料與工程,2014,43(11):2861~2864.[Deng Ying, Xiong Xiang, Zhang Yanhua, Tu Mingjing, Li Jing. State Key Laboratory for Powder Metallurgy, Central South University, Changsha 410083, China[J]. Rare Metal Materials and Engineering,2014,43(11):2861~2864.]
DOI:[doi]

復(fù)制
文章指標(biāo)
  • 點擊次數(shù):
  • 下載次數(shù):
  • HTML閱讀次數(shù):
  • 引用次數(shù):
歷史
  • 收稿日期:2013-11-05
  • 最后修改日期:
  • 錄用日期:
  • 在線發(fā)布日期: 2015-04-07
  • 出版日期: