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合金成分對Cu-Ni合金薄帶再結(jié)晶織構(gòu)形成的影響
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上海大學(xué)材料科學(xué)與工程學(xué)院,上海大學(xué)材料科學(xué)與工程學(xué)院

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TG166/TM26

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上海市“科技創(chuàng)新行動計劃”重大科技項目(11DZ1100303)


Effect of alloying elements on the formation of recrystallization texture of Cu-Ni alloy tapes
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School of Materials Science and Engineering, Shanghai University,School of Materials Science and Engineering, Shanghai University

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    摘要:

    采用冷坩堝懸浮熔煉技術(shù)冶煉了Cu-18at.%Ni、Cu-32at.%Ni、Cu-52at.%Ni和Cu-72at.%Ni四種合金鑄錠,鑄錠經(jīng)鍛造、熱軋、冷軋和再結(jié)晶退火,最終獲得了厚度為80 μm的薄帶。采用背散射電子衍射(EBSD)技術(shù)表征了合金再結(jié)晶織構(gòu),利用高分辨透射電鏡(HRTEM)分析了顯微組織結(jié)構(gòu)。結(jié)果表明,四種Cu-Ni合金冷軋后的形變織構(gòu)相似,但隨著合金薄帶中Ni含量增加,再結(jié)晶退火后立方織構(gòu)的份額減少,晶粒取向變得散亂,晶粒尺寸明顯變大;合金成分處于52-72at.%Ni范圍時,形變合金在回復(fù)階段的調(diào)幅分解是引起再結(jié)晶織構(gòu)散亂的主要原因,Cu-Ni 合金的單相固溶體是形變-再結(jié)晶后獲得立方織構(gòu)的關(guān)鍵因素。

    Abstract:

    Cu-xat.%Ni (x = 18,32,52,72) alloy were smelted by cold crucible induction levitation melting, and tapes with a final thickness of 80μm were obtained after forging, hot rolling, cold rolling and recrystallization annealing. The recrystallization texture and microstructure of alloy tapes were characterized by electron backscatter diffraction technology (EBSD) and high resolution transmission electron microscopy (HRTEM) respectively. The results showed that the deformation texture of these Cu-Ni alloys are similar, but with the increase of Ni content, the volume fraction of cube texture in alloy tapes decreased after recrystallization annealing, the grain orientation became scattered, and grain size significantly became larger. In the alloys with a composition of 52-72at.%Ni, spinodal decomposition occurred at recovery stage is the main cause of scattered recrystallization texture; single-phase solid solution of Cu-Ni alloy is the key element in obtaining cube texture after recrystallization.

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賀英,王均安.合金成分對Cu-Ni合金薄帶再結(jié)晶織構(gòu)形成的影響[J].稀有金屬材料與工程,2016,45(11):2975~2980.[He Ying, Wang Jun-an. Effect of alloying elements on the formation of recrystallization texture of Cu-Ni alloy tapes[J]. Rare Metal Materials and Engineering,2016,45(11):2975~2980.]
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  • 收稿日期:2014-08-28
  • 最后修改日期:2014-12-03
  • 錄用日期:2014-12-25
  • 在線發(fā)布日期: 2016-12-08
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