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半固態(tài)處理工藝參數(shù)對(duì)擠壓AZ91鎂合金微觀組織的影響
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中央高?;究蒲袠I(yè)務(wù)費(fèi)專題研究項(xiàng)目 (SWJTU11ZT30); 牽引動(dòng)力國(guó)家重點(diǎn)實(shí)驗(yàn)室基金項(xiàng)目; 國(guó)家自然科學(xué)基金 (51201142)


Effects of Semi-Solid Treatment Process Parameters on Microstructure of Extruded AZ91 Magnesium Alloy
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    摘要:

    研究了半固態(tài)等溫處理溫度和時(shí)間對(duì)擠壓AZ91鎂合金微觀組織演變的影響。擠壓AZ91鎂合金的微觀組織為流線帶狀組織,由分布于其間的細(xì)小再結(jié)晶α-Mg等軸晶組成。在半固態(tài)溫度區(qū)間進(jìn)行等溫處理時(shí),合金內(nèi)的低熔點(diǎn)相及溶質(zhì)元素富集區(qū)優(yōu)先開(kāi)始熔化,然后沿著晶界滲透,形成液相包圍固相晶粒的半固態(tài)組織。隨著等溫溫度的升高,固相晶粒熔化分離的速度加快。在等溫溫度為560 ℃時(shí),隨著等溫時(shí)間的延長(zhǎng),液相不斷增加,固相晶粒分離并不斷趨于圓整。等溫處理20 min后,合金達(dá)到了固/液平衡狀態(tài),Ostwald熟化機(jī)制開(kāi)始明顯,晶粒長(zhǎng)大成為主要機(jī)制。擠壓AZ91鎂合金較佳的等溫處理工藝為等溫溫度560 ℃,等溫時(shí)間20~30 min

    Abstract:

    The effects of semi-solid isothermal heat treatment temperature and holding time on microstructures evolution of extruded AZ91 magnesium alloy were studied. The microstructures of hot extrusion AZ91 magnesium alloy are characterized by streamline structure and small recrystallized α-Mg equiaxed grain. In the semi-solid isothermal treatment, the phase of low melting point begins to melt firstly, then permeates along the grain boundary, and finally the semi-solid structure which is liquid phase surrounded by solid-phase particles is formed. With the increase of isothermal temperature, melt and separation of the solid phases become faster. At the isothermal temperature of 560 oC, with the extension of isothermal holding time, the liquid phases increase obviously, solid phases separate and tend spheroid constantly. After holding for 20 min, the alloy reaches the solid-liquid equilibrium state, Ostwald ripening mechanism begins to be clear, and grains coarsening become the main mechanism. The better semi-solid processing technological parameters of extruded AZ91 alloy are 560 oC and 20~30 min

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王 棟,劉趙銘,張英波,權(quán)高峰.半固態(tài)處理工藝參數(shù)對(duì)擠壓AZ91鎂合金微觀組織的影響[J].稀有金屬材料與工程,2014,43(9):2277~2280.[Wang Dong, Liu Zhaoming, Zhang Yingbo, Quan Gaofeng. Effects of Semi-Solid Treatment Process Parameters on Microstructure of Extruded AZ91 Magnesium Alloy[J]. Rare Metal Materials and Engineering,2014,43(9):2277~2280.]
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  • 收稿日期:2013-09-29
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  • 在線發(fā)布日期: 2015-02-25
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