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新型高強(qiáng)鋁合金的熱變形行為及組織演變
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國家自然科學(xué)基金 (51175361); 山西省科技攻關(guān)項(xiàng)目 (20110321013-02); 山西省回國留學(xué)人員科研項(xiàng)目 (2011-074)


Hot Deformation Behavior and Microstructure Evolution of a New High Strength Aluminum Alloy
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    摘要:

    采用高溫壓縮實(shí)驗(yàn)研究了新型Al-Zn-Mg-Cu高強(qiáng)鋁合金在溫度300~450 ℃、應(yīng)變速率0.001~10 s-1和壓縮變形程度30%~80%范圍內(nèi)的熱變形行為和組織演變。分析了該合金在實(shí)驗(yàn)參數(shù)范圍內(nèi)變形的應(yīng)力-應(yīng)變曲線特征。動力學(xué)分析獲得該合金熱變形的應(yīng)力指數(shù)和激活能分別為4.97和150.07 kJ/mol, 表明合金的熱變形主要受擴(kuò)散所控制。金相組織觀察發(fā)現(xiàn),隨著變形溫度的升高或應(yīng)變速率的降低,變形組織晶內(nèi)析出相逐漸溶入基體組織,晶內(nèi)組織逐漸趨于均勻;同時粗大的晶粒沿變形方向拉長,晶界難溶相的碎化和彌散化程度增大。TEM和EBSD (electron back-scattered diffraction) 組織分析表明,該合金在高溫壓縮變形過程中組織演變主要是亞晶的形成和完善的過程,熱變形組織演變機(jī)理為動態(tài)回復(fù)和大應(yīng)變幾何動態(tài)再結(jié)晶

    Abstract:

    Hot deformation behavior and microstructure evolution of a new high strength Al-Zn-Mg-Cu alloy were studied in a temperatures range of 300~450 oC, a strain rates range of 0.001~10 s-1, and a reductions range of 30%~80% by high-temperature compression tests. Characteristics of stress-strain curves were investigated. Kinetics analyses indicate that the stress exponent and hot deformation activation energy are 4.97 and 150.07 kJ/mol, respectively, suggesting that deformation would be controlled by diffusion mainly. Microstructure observation by OM shows that precipitates in the deformed grain dissolve into the matrix and microstructure in the deformed grain become homogeneous gradually at higher temperatures or lower strain rates, while the prior coarse grains elongate along the deformation direction, and coarse un-dissolved phases at grain boundaries become smaller and more dispersive at the same time. The results of TEM and EBSD show that microstructure evolution during hot deformation of the alloy is characterized by generation and formation of sub-grains, and mechanisms of microstructure evolution during hot deformation is dynamic recovery and geometric dynamic recrystallization at large reductions.

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趙曉東,陶樂曉,王金亮,陳慧琴,劉建生.新型高強(qiáng)鋁合金的熱變形行為及組織演變[J].稀有金屬材料與工程,2014,43(9):2172~2176.[Zhao Xiaodong, Tao Lexiao, Wang Jinliang, Chen Huiqin, Liu Jiansheng. Hot Deformation Behavior and Microstructure Evolution of a New High Strength Aluminum Alloy[J]. Rare Metal Materials and Engineering,2014,43(9):2172~2176.]
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  • 收稿日期:2013-09-25
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