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靜態(tài)退火對(duì)Mg-Gd-Y-Zr擠壓合金的微結(jié)構(gòu)與織構(gòu)影響
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湖南工學(xué)院 先進(jìn)制造技術(shù)研究所,中南大學(xué) 材料科學(xué)與工程學(xué)院,湖南工學(xué)院,先進(jìn)制造技術(shù)研究所,湖南工學(xué)院,先進(jìn)制造技術(shù)研究所

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TG146.2

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湖南省自然科學(xué)基金項(xiàng)目 (11JJ4033);湖南省教育廳優(yōu)秀青年項(xiàng)目(12B030)


Effect of static annealing on microstructure and texture of Mg-Gd-Y-Zr extruded alloy
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Institute of Advanced Manufacturing Technology, Hunan Institute of Technology,School of Materials Science and Engineering, Central South University,Institute of Advanced Manufacturing Technology, Hunan Institute of Technology,Institute of Advanced Manufacturing Technology, Hunan Institute of Technology

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    摘要:

    本文研究了Mg-9Gd-4Y-0.6Zr擠壓合金在靜態(tài)退火過(guò)程中的微結(jié)構(gòu)與織構(gòu)的演變。采用金相顯微術(shù)、掃描電子顯微術(shù)、透射電子電子顯微術(shù)、差熱分析儀、XRD織構(gòu)測(cè)試儀及EBSD分析技術(shù)表征了合金的晶粒長(zhǎng)大、析出相沉淀及織構(gòu)改變。結(jié)果表明,退火初期的晶粒尺寸下降是由再結(jié)晶引起的;晶間不均勻變形誘發(fā)了晶間的局部析出,繼而抑制了再結(jié)晶過(guò)程??棙?gòu)分析表明,熱擠壓產(chǎn)生了常見的基面纖維織構(gòu)和不常見的柱面纖維織構(gòu),即c軸平行于擠壓方向;在靜態(tài)再結(jié)晶過(guò)程中,新晶粒形核會(huì)弱化柱面纖維,而晶粒長(zhǎng)大過(guò)程會(huì)強(qiáng)化柱面纖維。晶界與亞晶界上的大量析出相抑制了織構(gòu)改變。

    Abstract:

    The evolution of microstructure and texture for the Mg-9Gd-4Y-0.6Zr extruded alloy during static annealing was investigated. The grain growth, precipitation and texture modification were characterized by optical microscopy, scanning electron microscopy, transmission electron microscopy, differential scanning calorimeter, XRD texture instrument and EBSD. The results show that the recrystallization process resulted in the grain refinement at the initial stage of static annealing, and that the intergranular deformation stimulated local precipitating which in turn inhibited the recrystallization process. The texture analysis indicates that the hot extrusion produces the conventional basal fiber with {0001} // ED and the unusual prismatic fiber with c axis // ED. During static recrystallization, the process of grain nucleation weakens the prismatic fiber, while the process of grain growth strengthens it. A large number of plate phases precipitate at grain boundaries along with subgrain boundaries, which significantly inhibits the texture modification.

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李理,吳懿萍,吳遠(yuǎn)志,伍杰.靜態(tài)退火對(duì)Mg-Gd-Y-Zr擠壓合金的微結(jié)構(gòu)與織構(gòu)影響[J].稀有金屬材料與工程,2016,45(9):2263~2268.[Li Li, Wu YiPing, Wu Yuanzhi, Wu Jie. Effect of static annealing on microstructure and texture of Mg-Gd-Y-Zr extruded alloy[J]. Rare Metal Materials and Engineering,2016,45(9):2263~2268.]
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  • 收稿日期:2014-06-19
  • 最后修改日期:2014-09-22
  • 錄用日期:2014-11-20
  • 在線發(fā)布日期: 2016-10-09
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