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熱加工工藝對Ti-1300合金軋制棒材顯微組織的影響
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陜西省重點科技創(chuàng)新團隊計劃(2012KCT-23);陜西省科技統(tǒng)籌創(chuàng)新工程項目(2012KCTG04-04)


Effect of Heat Processing Technique on Microstructure of Ti-1300 Alloy
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    摘要:

    研究了軋制溫度、變形量以及熱處理工藝對Ti-1300合金顯微組織的影響,并討論了熱加工工藝與合金組織結(jié)構以及形貌之間的聯(lián)系規(guī)律。結(jié)果表明:兩相區(qū)軋制后的加工態(tài)Ti-1300合金主要由等軸的β相和球狀α相組成,隨軋制溫度向合金相變點溫度的升高,α相逐漸溶解在β基體上,因而β單相區(qū)軋制的合金主要由等軸的β相晶粒組成,而合金的晶粒隨變形量的增加而破碎越充分,組織也更加細小、均勻。兩相區(qū)固溶處理后的Ti-1300合金在晶界和晶間析出球狀以及條狀α相,彌散分布于亞穩(wěn)定β基體,產(chǎn)生細晶強化效應,而β單相區(qū)固溶處理后的合金主要由平均晶粒尺寸為60 μm的等軸β相組成。兩相區(qū)固溶處理后的時效態(tài)Ti-1300合金的組織主要由條狀初生αp相、針狀次生αs相以及β基體組成,熱軋溫度和變形量對時效態(tài)Ti-1300合金中αp相的形貌特征影響較小,但αp相和αs相都隨時效溫度的升高而不同程度的長大,針狀次生αs相彌散分布在β基體上。

    Abstract:

    The effects of rolling temperature, deformation degree and heat treatment on the microstructure of Ti-1300 alloy were studied with an emphasis on the relationship between the heat processing technique and microscopic structure. The results show that Ti-1300 alloy with rolling temperature under β-transus temperature is composed of spherical α phase and equiaxed β phase, and α phase dissolves into β matrix with increasing of the rolling temperature. When the rolling temperature is increased to β-transus temperature or higher, the equiaxed β phase becomes the only dominant phase. The grains of Ti-1300 alloy with large deformation can be greatly refined, and the structure becomes homogeneous. After α+β phase region solution treatment, α phase with sphericity or strip shape precipitate in grain boundary and intergranular position and then disperse in metastable β matrix, and lead to dispersion strengthening and fine grain strengthening; however, the alloy after β phase region solution treatment is mainly composed of equiaxed β phase with the average grain size of about 60 μm. The Ti-1300 alloy after aging treatment is composed of strip αp phase, acicular αs phase and β matrix. There is few influence of the heat processing technique on the morphology parameters of αp phase in Ti-1300 alloy after aging treatment, but the morphology of αp and αs phase grow up with the aging temperature increasing. Acicular αs phase is dispersed on the β matrix.

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盧金文,葛 鵬,趙永慶,李 倩,周 偉,洪 權.熱加工工藝對Ti-1300合金軋制棒材顯微組織的影響[J].稀有金屬材料與工程,2014,43(6):1441~1446.[Lu Jinwen, Ge Peng, Zhao Yongqing, Li Qian, Zhou Wei, Hong Quan. Effect of Heat Processing Technique on Microstructure of Ti-1300 Alloy[J]. Rare Metal Materials and Engineering,2014,43(6):1441~1446.]
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  • 收稿日期:2013-07-11
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  • 在線發(fā)布日期: 2014-11-13
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