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電場(chǎng)作用下SiC與Ti擴(kuò)散連接界面結(jié)構(gòu)及力學(xué)性能
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哈爾濱工業(yè)大學(xué),哈爾濱工業(yè)大學(xué)

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國(guó)家自然科學(xué)基金項(xiàng)目(面上項(xiàng)目,重點(diǎn)項(xiàng)目,重大項(xiàng)目)


Microstructure and mechanical properties of SiC/Ti diffusion bonding joints under electric field
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Harbin Industry of Technology,Harbin Industry of Technology

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    摘要:

    在擴(kuò)散連接過(guò)程中施加電壓,會(huì)對(duì)材料內(nèi)部離子的遷移過(guò)程產(chǎn)生一定的影響,從而影響材料的組織和性能。本文在施加電壓下對(duì)SiC與Ti進(jìn)行了擴(kuò)散連接。研究發(fā)現(xiàn),當(dāng)金屬、陶瓷分別連接電場(chǎng)正、負(fù)極時(shí),電場(chǎng)極大促進(jìn)界面擴(kuò)散層厚度增加,而電壓反接時(shí)促進(jìn)作用明顯減弱。SiC與Ti的擴(kuò)散界面反應(yīng)過(guò)程中,界面處產(chǎn)生了Ti5Si3和TiC新相,界面結(jié)構(gòu)從SiC到Ti為SiC/TiC/(Ti5Si3 TiC)/Ti。性能測(cè)試結(jié)果表明,1000℃/2h/7.5MPa時(shí)接頭剪切強(qiáng)度為66.4MPa,950℃/1.5h/7.5MPa/400V時(shí)接頭剪切強(qiáng)度為69.6MPa,即施加電壓進(jìn)行連接時(shí),在不降低接頭性能的同時(shí)提高了連接效率。

    Abstract:

    In the process of heat treatment, the electric field has a certain effect on the migration of ions inside materials, thus affecting the organization and performance of the material. In this paper, diffusion bonding SiC to Ti was carried out by applying voltage. Study shows that, when the metal and ceramic connect the positive and negative of the electric field respectively, the electric field will promote the increase of the thickness of interface diffusion layer, but reversed connection can weaken the promotion of interface diffusion layer thickening significantly. In the process of SiC/Ti interface diffusion reaction, new phase Ti5Si3 and TiC generate at the interface, and the interface structure from SiC to Ti is SiC/TiC/(Ti5Si3 TiC)/Ti. Mechanical properties testing results show that the shear strength of the joint at 1000℃/2h/7.5MPa is 66.4MPa, but the shear strength of the joint at 950℃/1.5h/7.5MPa/400V is 69.6MPa, so applying voltage during the bonding process can keep the shear strength and, as the same time, improve the efficiency of the bonding.

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王清,孫東立.電場(chǎng)作用下SiC與Ti擴(kuò)散連接界面結(jié)構(gòu)及力學(xué)性能[J].稀有金屬材料與工程,2016,45(7):1749~1754.[Wang Qing, Sun Dongli. Microstructure and mechanical properties of SiC/Ti diffusion bonding joints under electric field[J]. Rare Metal Materials and Engineering,2016,45(7):1749~1754.]
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  • 收稿日期:2014-06-01
  • 最后修改日期:2015-01-09
  • 錄用日期:2015-02-06
  • 在線發(fā)布日期: 2016-10-09
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