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FGH96高溫合金的再結(jié)晶組織特征
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西北工業(yè)大學(xué)

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TG113

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中國博士后科學(xué)基金;國家自然科學(xué)基金項(xiàng)目(面上項(xiàng)目,重點(diǎn)項(xiàng)目,重大項(xiàng)目)


Recrystallization Characterization of FGH96 Superalloy
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Northwestern Polytechnical University

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    摘要:

    FGH96高溫合金的再結(jié)晶主要包括孕育期、形核期和晶核長大期。再結(jié)晶形核與長大對溫度非常敏感:當(dāng)變形量較小時,即在1050℃溫度下充分形核,在1080℃溫度下再結(jié)晶晶核等軸化過程穩(wěn)定,能夠得到均勻細(xì)小的等軸晶,而當(dāng)溫度高于1110℃時,再結(jié)晶等軸晶粒顯著長大;隨著變形量的增大,獲得細(xì)晶粒的溫度由1110℃降低到1080℃左右。促進(jìn)形核、抑制晶粒長大均有利于晶粒細(xì)化。另外,再結(jié)晶優(yōu)先在原始顆粒邊界發(fā)生,當(dāng)變形不充分時,內(nèi)部殘留未再結(jié)晶區(qū),得到不完全再結(jié)晶組織,即“項(xiàng)鏈”組織。同時,這種組織也是粉末冶金材料晶粒細(xì)化過程中必然存在的中間態(tài)特征組織,隨著變形方向的增加、累積變形量的增大,原始顆粒中心區(qū)域能夠發(fā)生再結(jié)晶,“項(xiàng)鏈”組織也逐漸轉(zhuǎn)化成等軸細(xì)晶組織。

    Abstract:

    The recrystallization of powder metallurgy superalloy FGH96 undergoes three characteristic periods, viz., incubation, nucleation and growth period. The recrystallization behavior is sensitive to annealing temperature. When the temperature is 1050℃, there is lots of nucleation at the previous particle boundaries. The nucleation grow up and the fine equiaxed grains are obtained when the temperature is 1080℃. However, the equiaxed grains would be significantly getting coarse when the temperature is1110℃. Recrystallization usually takes place at previous particle boundaries during hot deformation process. When the deformation is not enough, a typically incomplete recrystallization microstructure, named the necklace microstructure, will be obtained. The necklace microstructure has fine equiaxed grains inlayed in non-equiaxed coarse grains surronding. Meanwhile, it is also the intermediate microstructure during the refinement processing of the PM materials. Both the severe total deformation and multiple deformation direction are favorable for grain refinement.

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寧永權(quán). FGH96高溫合金的再結(jié)晶組織特征[J].稀有金屬材料與工程,2016,45(5):1225~1229.[Ning Yongquan. Recrystallization Characterization of FGH96 Superalloy[J]. Rare Metal Materials and Engineering,2016,45(5):1225~1229.]
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  • 收稿日期:2014-05-06
  • 最后修改日期:2014-06-06
  • 錄用日期:2015-10-13
  • 在線發(fā)布日期: 2016-06-02
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