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固溶溫度對Al-11.7Zn-2.2Mg-2.0Cu-0.12Zr鋁合金組織及性能的影響
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北京航空材料研究院,北京航空材料研究院,北京航空材料研究院,北京航空材料研究院

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Effect of solution temperature on the properties and microstructure of a Al-11.7Zn-2.2Mg-2.0Cu-0.12Zr aluminum alloy
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Beijing Institute of Aeronautical Materials,Beijing Institute of Aeronautical Materials,Beijing Institute of Aeronautical Materials,Beijing Institute of Aeronautical Materials

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    摘要:

    采用拉伸試驗(yàn)機(jī)、金相顯微鏡、XRD、SEM以及EMPA等手段對合金總含量超過15 wt.%的新型超高強(qiáng)鋁合金不同固溶溫度處理后的組織與性能變化規(guī)律進(jìn)行了研究。結(jié)果表明:晶內(nèi)的固溶度隨溫度升高逐漸增加,在474℃時(shí)基本達(dá)到穩(wěn)定狀態(tài),此時(shí),約有99 wt.%的Zn、Mg以及75 wt.%的Cu溶入晶內(nèi),其余的合金元素富集在晶界第二相內(nèi),此時(shí)第二相主要由含Cu的T相構(gòu)成;合金最佳固溶溫度為474℃,此時(shí)合金的抗拉強(qiáng)度為688 MPa、延伸率為8 %;溫度為476℃時(shí),合金局部區(qū)域出現(xiàn)輕微過燒,導(dǎo)致延伸率迅速降低;斷口分析顯示,隨固溶溫度的提高,再結(jié)晶程度增加,晶界第二相數(shù)量減少,合金的拉伸斷口由較低溫度時(shí)的沿晶+穿晶混合斷口轉(zhuǎn)變?yōu)檩^高溫度時(shí)的沿晶斷口為主。

    Abstract:

    Effect of solution temperature on solid solubility, tensile properties, microstructure and fractography of a new Al-Zn-Mg-Cu-Zr aluminum alloy were studied by tensile testing, optical microscopy, XRD, SEM and EPMA. The results indicated that the solid solubility of matrix increase with the increasing temperature, and when it reach stable state at 474℃, about 99 wt.%Zn, Mg and 75 wt.%Cu enter matrix, the residual elements enrichment in the second phase particles(T phase)located on grain boundary. The optimal solution temperature is 474℃, the tensile strength of forge can get up to 688MPa, and elongation is 8%. At 476℃, the slight over-burned in local region is observed, which lead to the decrease of elongation rapidly. It is found that the tensile fractography was affected by the volume fraction of residual particles and the recrystallization level of deformed grains. With the temperature increasing, the fractography transform from intergranular cracking mixed dimple-type transgranular cracking to intergranular cracking.

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李國愛,張坤,陸政,何維維.固溶溫度對Al-11.7Zn-2.2Mg-2.0Cu-0.12Zr鋁合金組織及性能的影響[J].稀有金屬材料與工程,2016,45(4):1040~1044.[liguoai, zhangkun, luzheng, heweiwei. Effect of solution temperature on the properties and microstructure of a Al-11.7Zn-2.2Mg-2.0Cu-0.12Zr aluminum alloy[J]. Rare Metal Materials and Engineering,2016,45(4):1040~1044.]
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  • 收稿日期:2014-05-06
  • 最后修改日期:2014-05-30
  • 錄用日期:2014-09-28
  • 在線發(fā)布日期: 2016-06-02
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