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電渣重熔連續(xù)定向凝固Rene88DT合金組織與偏析行為
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鋼鐵研究總院

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國家自然科學(xué)基金資助(50735001,50675089,50975127)


Structure and segregation behavior of Rene88DT alloy prepared by ESR-CDS?
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Central Iron and Steel Research Institute

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    摘要:

    利用電渣重熔連續(xù)定向凝固技術(shù)(ESR-CDS)成功制備了Rene88DT高溫合金鑄錠。借助于金相顯微鏡,帶有能譜的掃描電鏡以及透射電鏡,對電渣重熔連續(xù)定向合金Rene88DT鑄錠進行分析,并與傳統(tǒng)電渣鑄錠進行了對比。研究結(jié)果顯示,電渣重熔連續(xù)定向凝固合金Rene88DT鑄錠消除了最為嚴(yán)重的中心偏析,中心偏析在傳統(tǒng)電渣鑄錠中是普遍存在的,這種偏析存在于柱狀晶與等軸晶交界處或者柱狀晶之間相互交界面處。此外,電渣重熔連續(xù)定向凝固合金二次枝晶間距較傳統(tǒng)電渣鑄錠小,析出相尺寸也較小。由于微觀偏析程度的降低,使得合金在經(jīng)過1200℃/24h后的熱處理即可達(dá)到均勻化效果。夾雜物統(tǒng)計結(jié)果顯示,電渣重熔連續(xù)定向凝固合金夾雜物最大尺寸為5.89微米,與傳統(tǒng)電渣合金和粉末合金相比夾雜物數(shù)量降低60%。電渣重熔連續(xù)定向凝固合金宏觀偏析和夾雜物水平的降低可提高熱加工塑性,為鑄&鍛工藝實施提供基礎(chǔ)。

    Abstract:

    Abstract:Directionally solidified Rene88DT superalloy ingots were successfully produced by electroslag remelting continuous directional solidification (ESR-CDS) technology. Compared with conventional ESR ingot, the as-cast structures of ESR-CDS Rene88DT alloy ingot were analyzed using by optical microscopy (OM)、field emission scanning electron microscopy (FESEM) with energy spectrum and transmission electron microscopy(TEM). The results showed that the ESR-CDS Rene88DT alloy ingot eliminated the region of the severe central segregation which existed commonly in the conventional ESR ingot because of the formation of intersection of interfaces between columnar crystal and equiaxed crystal or columnar crystal each other. In addition, the ESR-CDS Rene88DT alloy ingot showed smaller secondary dendritic spacing, smaller non-equilibrium precipitates phase. Due to the decreasing micro-segregation level, uniform distribution of alloy elements can be achieved when subjected to the heat treatment at 1200 oC for 24h. Statistical results of inclusions revealed that the maximum size of inclusion in the ESR-CDS Rene88DT alloy was not more than 5.89μm and the inclusion volume reduced by 60% compared with conventional ESR and P/M respectively. The hot working plasticity of directionally solidified Rene88DT superalloy can be improved, which makes a basis for implementation of cast-and-wrought (C&W) route.

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李福林.電渣重熔連續(xù)定向凝固Rene88DT合金組織與偏析行為[J].稀有金屬材料與工程,2016,45(6):1437~1442.[lifulin. Structure and segregation behavior of Rene88DT alloy prepared by ESR-CDS?[J]. Rare Metal Materials and Engineering,2016,45(6):1437~1442.]
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  • 收稿日期:2014-04-20
  • 最后修改日期:2014-11-21
  • 錄用日期:2014-12-25
  • 在線發(fā)布日期: 2016-10-08
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