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再結(jié)晶退火工藝對Ni5W合金長帶織構(gòu)的影響
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國家自然科學(xué)基金(51171002);北京市自然科學(xué)基金(2132011);博士點(diǎn)基金(20121103110012);北京市重點(diǎn)項(xiàng)目B類(KZ201310005003);北京市屬高等學(xué)校創(chuàng)新團(tuán)隊(duì)建設(shè)計(jì)劃項(xiàng)目(IDHT20130510)


Effect of Recrystallization Annealing on Texture Evolution of Ni5W Alloy Trip
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    摘要:

    采用中頻感應(yīng)熔煉方法制備Ni-5at%W合金錠,經(jīng)鍛造和熱軋后,再冷軋到50 m長,厚度為60 μm的帶材。隨后在800~1200 ℃進(jìn)行再結(jié)晶退火處理。在兼顧“高織構(gòu)”和“淺晶界”要求下,得出1100 ℃/0.5 h是Ni5W合金基帶最佳的退火工藝。根據(jù)X射線衍射(XRD)和電子背散射衍射技術(shù)(EBSD)結(jié)果,在1100 ℃/0.5 h時(shí)該Ni5W合金基帶的再結(jié)晶立方織構(gòu)含量達(dá)到98.9%(≤10°),且晶粒尺寸均勻。退火后的Ni5W合金基帶掃描半高寬(FWHM)值和孿晶界含量接近德國Dresden公司商業(yè)化Ni5W合金基帶的水平

    Abstract:

    A Ni-5at%W ingot was prepared by medium frequency induction melting. The ingot was forged, hot-rolled and cold-rolled into trips with 60 μm thickness and 50 m length. Recrystallization annealing for the substrate trip was carried out at different temperatures (800~1200 °C) for different time. Taking account of high cube texture and shallow boundary, the recrystallization annealing of 1100 °C/0.5 h is regarded as the best. According to X-ray diffraction and EBSD analyses, the cube grain content of the tape annealed at 1100 °C for 0.5 h reaches as high as 98.9% (tolerance angle of less than 10°), and grain size is uniform. The FWHM values of the in-plane and the content of crystal twin are slightly different from that of the commercial Ni5W tape supplied by Germany Dresden

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王 毅,索紅莉,馬 麟,王建宏,李孟曉,孟易辰,劉 敏.再結(jié)晶退火工藝對Ni5W合金長帶織構(gòu)的影響[J].稀有金屬材料與工程,2013,42(12):2590~2593.[Wang Yi, Suo Hongli, Ma Lin, Wang Jianhong, Li Mengxiao, Meng Yichen, Liu Min. Effect of Recrystallization Annealing on Texture Evolution of Ni5W Alloy Trip[J]. Rare Metal Materials and Engineering,2013,42(12):2590~2593.]
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  • 收稿日期:2012-12-14
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