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放電等離子燒結(jié)TaC/Ti復(fù)合材料的組織與力學(xué)性能
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Microstructure and Mechanical Properties of TaC/Ti Composite Prepared by SPS
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    摘要:

    采用放電等離子燒結(jié)(SPS)制備碳化鉭(TaC)顆粒增強鈦基復(fù)合材料,通過X射線衍射儀、掃描電鏡和電子探針分析了復(fù)合材料的微觀組織和力學(xué)性能。結(jié)果表明:SPS制備方法在溫度高于800 ℃燒結(jié)可得到致密TaC/Ti復(fù)合材料;TaC顯著提高鈦的硬度和強度,加入5%TaC復(fù)合材料的維氏硬度高于500 MPa,抗彎強度高于600 MPa;燒結(jié)過程中發(fā)生固相擴散反應(yīng),TaC與金屬鈦反應(yīng)被消耗,析出分布均勻的(Ti,Ta)C1-x碳化物,分解出的Ta固溶于鈦金屬基體;第二相強化與固溶強化2種強化機制的共同作用使復(fù)合材料強度、硬度大幅度提高

    Abstract:

    Tantalum carbide (TaC) particles reinforced titanium composites were prepared by sparking plasma sintering (SPS). Microstructure and mechanical properties were analyzed by X-ray diffraction, scanning electron microscope and electron probe. The results show that densified TaC/Ti composite can be obtained when sintering above 800 ℃ by SPS. The hardness and strength of titanium can be significantly improved by adding TaC. The hardness of samples with 5%TaC addition are higher than 500 MPa and the bending strength are higher than 600 MPa. The original TaC was consumed owing to solid phase diffusion and reaction in the sintering process;. A new phase of (Ti, Ta)C1-x carbide was formed, which distributed uniformly around titanium matrix. The tantalum has been found in titanium matrix, which means solid solution is formed. The great improvement of the composite strength is associated with phase strengthening and solution strengthening mechanism

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楊西亞,郭玉忠,陳昱潼,淡露露,王劍華.放電等離子燒結(jié)TaC/Ti復(fù)合材料的組織與力學(xué)性能[J].稀有金屬材料與工程,2013,42(11):2274~2278.[Yang Xiya, Guo Yuzhong, Chen Yutong, Dan Lulu, Wang Jianhua. Microstructure and Mechanical Properties of TaC/Ti Composite Prepared by SPS[J]. Rare Metal Materials and Engineering,2013,42(11):2274~2278.]
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  • 收稿日期:2012-11-05
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