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稀土元素Gd、Nd對(duì)AZ80鎂合金組織和力學(xué)性能的影響
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國家自然科學(xué)基金(50875031);航空科學(xué)基金(20095263005)


Effects of Rare-Earth Elements Gd and Nd on Microstructure and Mechanical Properties of AZ80 Magnesium Alloy
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    摘要:

    通過金相、掃描電鏡、電子探針和力學(xué)性能測(cè)試等方法研究了稀土元素Gd和Nd對(duì)AZ80鎂合金鑄態(tài)和擠壓態(tài)組織和力學(xué)性能的影響。結(jié)果表明,適當(dāng)添加稀土元素可以使AZ80鎂合金的鑄態(tài)樹枝晶基本消失,晶界處層片狀Mg17Al12相增多。均勻化后晶粒尺寸明顯減小。合金經(jīng)擠壓后均發(fā)生了動(dòng)態(tài)再結(jié)晶,動(dòng)態(tài)析出的β相沿著再結(jié)晶晶粒的晶界分布。加入2%RE(Gd,Nd)后,析出相阻礙再結(jié)晶晶粒長大和粒子激發(fā)形核再結(jié)晶共同作用起到了細(xì)晶強(qiáng)化的效果,且高硬質(zhì)Al2Gd和Al2Nd相能有效阻礙位錯(cuò)運(yùn)動(dòng)從而大幅度提高了合金的屈服強(qiáng)度。隨著RE(Gd,Nd)含量的增多,β相析出減少,稀土相顆粒變大,弱化了動(dòng)態(tài)再結(jié)晶效果,導(dǎo)致應(yīng)力集中,強(qiáng)度下降。當(dāng)加入2%RE(Gd,Nd)時(shí)其抗拉強(qiáng)度最大,綜合性能較好。

    Abstract:

    The effects of Gd and Nd addition on microstructures and tensile properties of as-cast and extruded AZ80 magnesium alloy was investigated using OM, SEM, EPMA and mechanical property tests. The results show that the appropriate rare earth elements can improve the microstructures of as-cast AZ80 magnesium alloy with dendrite disappearing and more Mg17Al12 lamellar phase appearing along the grain boundaries. Grain size is reduced after homogenization. Dynamic recrystallization (DRX) occurs after extrusion and dynamically precipitated β phase distributes along the recrystallized grain boundaries in all the alloys. When adding 2% RE (Gd, Nd), the precipitated β phase hinders the grain growth and particle stimulated nucleation plays a common role in fine-grain strengthening. The highly rigid Al2Gd and Al2Nd phase can effectively impede dislocation movement and thus improve the yield strength. With the increase of RE (Gd, Nd) content, β phase precipitation decreases, RE phase particles become larger which weakens the effect of dynamic recrystallization and leads to stress concentration and strength decrease. The maximum tensile strength and best comprehensive performance can be achieved by adding 2% RE(Gd, Nd).

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朱 瓊,房燦峰,李乃樸,孟令剛,王 宇,吳友芳,張興國.稀土元素Gd、Nd對(duì)AZ80鎂合金組織和力學(xué)性能的影響[J].稀有金屬材料與工程,2013,42(4):771~775.[Zhu Qiong, Fang Canfeng, Li Naipu, Meng Linggang, Wang Yu, Wu Youfang, Zhang Xingguo. Effects of Rare-Earth Elements Gd and Nd on Microstructure and Mechanical Properties of AZ80 Magnesium Alloy[J]. Rare Metal Materials and Engineering,2013,42(4):771~775.]
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  • 收稿日期:2012-04-30
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