超位錯可由 {111} 面交滑移到 {100} 面,形成K-W鎖,而切過γ′相的<110>超位錯在 {111} 面發(fā)生分解,可形成 (1/3)<112> 超肖可萊不全位錯+層錯的位錯組態(tài),阻礙位錯運動和抑制位錯的交滑移"/>

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一種含Re單晶鎳基合金的中溫蠕變行為及影響因素
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國家自然科學基金項目 (50571070)和教育部博士點基金 (20092102110003)


Creep Behavior and Its Effect Factors of a Single Crystal Nickel-Based Superalloy Containing 4.5%Re at Medium Temperature
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    摘要:

    通過對合金進行不同溫度的固溶處理、蠕變曲線測定及組織形貌觀察,研究了熱處理工藝對4.5%Re鎳基單晶合金中溫蠕變行為的影響。結果表明:隨著固溶溫度提高,可降低元素的偏析程度,提高合金的蠕變性能。在760 ℃/800 MPa條件的蠕變期間,合金中γ′相不形成筏狀組織,但在近斷口區(qū)域,立方γ′ 相的扭曲程度增加。合金在蠕變期間的變形特征是位錯在基體中運動和剪切γ′相,其中,切入γ′ 相的<110>超位錯可由 {111} 面交滑移到 {100} 面,形成K-W鎖,而切過γ′相的<110>超位錯在 {111} 面發(fā)生分解,可形成 (1/3)<112> 超肖可萊不全位錯+層錯的位錯組態(tài),阻礙位錯運動和抑制位錯的交滑移

    Abstract:

    The influence of heat treatment techniques on medium temperature creep behaviors of the 4.5%Re single crystal nickel-base superalloy with different heat treatment regimes was investigated by means of creep curve measurement and microstructure observation. Results show that the creep property of the alloy is obviously improved with enhancing the solution temperature due to decreasing the segregation extent of the elements. After fully heat treated, the microstructure of the alloy consists of the cubic g¢ phase embedded coherent in the g matrix. During creep under the condition of 760 °C/800 MPa, no rafted structure of g¢ phase is detected, but the twisted configuration of the g¢ phase is formed in the regions near the fracture. In the ranges of the applied stresses and temperatures, the alloy displays a better creep resistance and a longer creep lifetime. And the deformation features of the alloy during creep are that the dislocations move in the g matrix channels and shear into the g¢ phase, the <110> super-dislocation shearing into the g¢ phase can be cross-slipped from {111} planes to {100} planes to form K-W locking, or the <110> super-dislocation shearing into the g¢ phase is decomposed to form the configuration of (1/3)<112> super-Shockleys partials plus the stacking fault, which may hinder dislocations movement and restrain the cross-slipping of dislocations. This is thought to be the main reason of the alloy having a better creep resistance

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田素貴,曾 征,張 超,劉 臣,李柏松.一種含Re單晶鎳基合金的中溫蠕變行為及影響因素[J].稀有金屬材料與工程,2013,42(3):494~499.[Tian Sugui, Zeng Zheng, Zhang Chao, Liu Chen, Li Bosong. Creep Behavior and Its Effect Factors of a Single Crystal Nickel-Based Superalloy Containing 4.5%Re at Medium Temperature[J]. Rare Metal Materials and Engineering,2013,42(3):494~499.]
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  • 收稿日期:2012-03-30
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