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TA15鈦合金雙重熱處理工藝及其微觀組織演化的EBSD研究
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EBSD Study on Dual Heat Treatment and Microstructure Evolution of TA15 Titanium Alloy
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    摘要:

    針對航空航天工業(yè)中廣泛應用的近a TA15鈦合金,開展了不同熱處理參數下的雙重熱處理實驗研究。利用背散射電子技術(Electronic backscatter diffraction, EBSD)表征了不同熱處理參數下微觀組織形貌特征和晶體學取向分布及規(guī)律。對比分析了熱處理處保溫時間對微觀組織形貌及取向分布的影響規(guī)律。揭示了雙重熱處理過程中球化的等軸晶粒,條狀次生as晶粒及b轉變組織的形成演化過程;分析了不同組織間的晶體取向與位置分布關系。研究表明:雙重熱處理過程中一次保溫時間對等軸初生ap形貌及分布等影響較大;熱處理過程中球化的等軸晶粒來源于未轉變的ap 相;二次保溫時間對as形貌、尺寸等具有顯著影響;二次保溫過程中細條狀as表現為先增長再增厚的生長模式;ap與相鄰的as晶體學取向關系表現出一定的統(tǒng)計性規(guī)律。

    Abstract:

    The study of dual heat treatment with different parameters has been performed on TA15 titanium alloy, which is a typical near a titanium and widely used in aerospace. The Electronic backscatter diffraction (EBSD) technique has been employed to characterize the microstructure and analyze the crystal orientation distribution of those samples subjected to different heat treatment. The effect of the heat holding time on microstructure morphology and orientation distribution was investigated. The formation and evolution of equiaxed primary ap, lamellar second as and transformed bT during the process of dual heat treatment has been revealed. The crystal orientation relationship between the ap and adjacent as has been analyzed. The results indicate that the holding time of stage I has an obvious influence on the morphology and distribution of ap. The equiaxed ap comes from heat treatment stage I as a result of retained primary ap. The holding time of stage II has a significant effect on the size and morphology of as. The mode of first lengthening and then thickening has been observed during the as coarsening process. A certain degree of match has been found between the crystal orientation of ap and adjacent as.

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朱景川,何 東,楊夏煒,劉 勇. TA15鈦合金雙重熱處理工藝及其微觀組織演化的EBSD研究[J].稀有金屬材料與工程,2013,42(2):382~386.[Zhu Jingchuan, He Dong, Yang Xiawei, Liu Yong. EBSD Study on Dual Heat Treatment and Microstructure Evolution of TA15 Titanium Alloy[J]. Rare Metal Materials and Engineering,2013,42(2):382~386.]
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  • 收稿日期:2012-02-11
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