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壓鑄鎂合金AM60B的微觀組織特征
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國家高技術(shù)研究發(fā)展計(jì)劃項(xiàng)目(2009AA03Z114);國家科技重大專項(xiàng)項(xiàng)目(2011ZX04014-052);日本東洋機(jī)械金屬株式會(huì)社國際合作項(xiàng)目(083000148)


Microstructure Characteristics of High Pressure Die Cast AM60B Magnesium Alloy
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    摘要:

    鎂合金壓鑄件中的壓室預(yù)結(jié)晶組織及離異共晶組織對(duì)鑄件最終使用性能有著重要的影響。針對(duì)冷室壓鑄工藝,采用AM60B鎂合金研究不同低速速度及高速速度下壓鑄實(shí)驗(yàn)件的凝固組織特征。通過OM、EBSD、XRD、SEM及EDS等實(shí)驗(yàn)手段進(jìn)行分析和定量統(tǒng)計(jì)。結(jié)果表明:在低速壓射階段,壓室中熔體的過熱度消失,達(dá)到初生相形核條件;在高速充填型腔過程中,壓室預(yù)結(jié)晶組織向鑄件中心偏聚,使得其心部含量高于表層;同時(shí),壓鑄件靠近澆口端壓室預(yù)結(jié)晶組織含量高于遠(yuǎn)離澆口端;低速速度越小,壓鑄件中壓室預(yù)結(jié)晶組織含量越高;高速速度越小,壓鑄件中壓室預(yù)結(jié)晶顆粒越粗大,枝晶形貌越完整。在壓鑄凝固后期,初生α-Mg晶界處出現(xiàn)離異共晶組織,共晶β-Mg17Al12相在壓鑄件中心及表層分別呈網(wǎng)狀和粒狀分布,且壓鑄件中心及缺陷帶位置的共晶組織含量高于表層。

    Abstract:

    The externally solidified crystals (ESCs) and divorced eutectics in die castings of magnesium alloy have a great influence on the final performance of castings. Under the cold-chamber high pressure die casting (HPDC) process, samples were produced at different slow shot phase and fast shot phase plunger velocities to investigate the microstructure characteristics of AM60B magnesium alloy. Based on the analysis and statistics of the experimental results obtained by using OM, EBSD, XRD, SEM and EDS, it is concluded that at the slow shot phase of the HPDC process, nucleation and crystals growth occur in the melt in the shot sleeve due to the loss of superheat; the ESCs are migrating to the central region of the castings during the fast shot phase of the melt into the die cavity at high speed, which lead to a higher distribution of the ESCs at the central region than the surface layer of the castings. Besides, the percentage of the ESCs is higher at a lower slow shot phase plunger velocity, and also is higher at the area near the gate than that of the area far from the gate of the castings. Coarse dendrites are observed at the cross section of the castings at a lower fast shot phase plunger velocity. At the last stage of solidification under HPDC process, fully divorced eutectics consisting of α-Mg and β-Mg17Al12 appear at the grain boundary of the primary α-Mg. Islands of β-Mg17Al12 phase are observed at the central region of the castings, while the β-Mg17Al12 phase reveals a more dispersed and granular morphology at the surface layer. The percentage of the eutectics is higher at the central region than that at the surface layer of the castings, whilst the defect band also contains a higher percentage of the eutectics than those at the adjacent regions.

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吳孟武,熊守美.壓鑄鎂合金AM60B的微觀組織特征[J].稀有金屬材料與工程,2012,41(9):1580~1585.[Wu Mengwu, Xiong Shoumei. Microstructure Characteristics of High Pressure Die Cast AM60B Magnesium Alloy[J]. Rare Metal Materials and Engineering,2012,41(9):1580~1585.]
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  • 收稿日期:2011-09-20
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