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鉬鑭合金板材料舟的研制及其斷裂行為分析
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Preparation of La-doped Molybdenum Boat and Analysis on Fracture Behavior
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    摘要:

    研究摻雜稀土鑭的鉬粉經(jīng)壓型、燒結(jié)、交叉換向軋制而成的鉬鑭合金板熱沖壓鉬舟變溫變載下的力學行為,探討高溫退火后析出物的彌散分布對鉬鑭合金板材力學性能的影響及加熱制度對合金板材沖壓成型性能的影響,分析料舟的斷裂機制。研究表明,彌散分布的La2O3明顯提高了鉬板再結(jié)晶溫度與力學性能,交叉軋制降低了板材縱向和橫向力學性能的差異,有利于鉬鑭合金板的沖壓成型;對2.8 mm厚Mo-1.0%La2O3合金板及沖壓模具在550 ℃進行加熱,將得到最大的沖壓變形量;鉬舟在18管爐內(nèi)承受變溫變載荷長期運行后,由于材料內(nèi)部的空位遷移與滑移面上的位錯滑移導致的韌窩撕裂,使料舟最終發(fā)生了宏觀斷裂。

    Abstract:

    La2O3 doped Mo powder was pressed, sintered and cross rolled to prepare alloy plates. Then the plates were stamped to obtain molybdenum boat. The mechanical properties of the molybdenum boat were investigated under the condition of variable temperatures and loads. The influences of precipitate dispersive distribution on the mechanical properties and the influence of heating system on the stamping property were discussed for the alloy plates. And the fracture mechanism of the boat was analyzed. Results show that La2O3 of dispersive distribution increases markedly the recrystallization temperature and mechanical properties of the Mo plates. Cross rolling decreases the difference of mechanical properties between transversal and longitudinal directions, which is favorable for the stamping of Mo-La2O3 alloy plates. The maximum punch deformation can be reached when heating the 2.8 mm thick Mo-10%La2O3 alloy plate and stamping dies at 550 oC. After long-time operation of the boat in 18-tube furnace under the variable temperature and load condition, it is found that vacancy migration and dislocation slip result in dimple tear, and eventually lead to the macroscopic fracture of the molybdenum boat.

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韓 強.鉬鑭合金板材料舟的研制及其斷裂行為分析[J].稀有金屬材料與工程,2012,41(9):1564~1567.[Han Qiang. Preparation of La-doped Molybdenum Boat and Analysis on Fracture Behavior[J]. Rare Metal Materials and Engineering,2012,41(9):1564~1567.]
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  • 收稿日期:2011-09-28
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